تحضير رقائق الكرافين النانوية و دراسة خواصها التركيبية

الملخص EN

The grapheme Flakes were prepared by reduction graphite oxide which was prepared by Hummer’s method.

X-ray diffraction (XRD) pattern showed that the graphene oxide have a sharp peak at (001) with d-spacing d001= 7.4Å at angle 2ϴ=11.85˚and graphene has broad peak at (002) with d-spacing d002=3.4Å at angle 2ϴ= 25.72˚ with lattice constant (a=2.47 Å).

The particle size was calculated by using equation Debye - Scherer and Williamson - Hall equations, Scanning electron microscopy examination and particle size analyzer proved that the graphene Flakes were in nano size.

Also the surface area of nanoparticles showed a value 270 m2/g .

The micrographs of (scanning electron microscopy) showed that graphene oxide has a fluffy aggregation and the form of graphene as a flakes or nano-sheets.