Synthesis and characterization of some transition metals complexes with 1, 2-bis-[3-(phenyl amino)-5-imino-1, 2, 4 thiadiazolyl] ethene
Joint Authors
al-Bayati, Rida Ibrahim
al-Ubaydi, Najat J.
al-Jabburi, Mahmud Najm Abd
Source
Issue
Vol. 2006, Issue 22 (30 Jun. 2006), pp.243-249, 7 p.
Publisher
University of Babylon College of Sciences
Publication Date
2006-06-30
Country of Publication
Iraq
No. of Pages
7
Main Subjects
Abstract AR
نظرا للأهمية البايولوجية و الصناعية لمشتقات 4,2,1-ثاياديازول فقد تم في هذا البحث تحضير قاعدة شيف جديدة بالتفاعل التكثيفي لمعوض 3- فنيل امينو-5-امينو -4,2,1-ثاياديازول مع الكلايوكسال.
قد استخدم هذا الليكند للتعقيد مع بعض العناصر الانتقالية وهي , Cu(II) , Zn(II) ,Cd(II) , Hg(II) , Cr(III) , Mn(II) , Ni(II) , ثم دراسة و تشخيص الليكند و معتقداته و بواسطة التحليل الدقيق للعناصر C.H.N.M)) و الطرق الطيفية FT.I.R)) و UV-Vis)) و قياس التوصيلية المولارية عند تركيز 10ֿ³ مولاري في مذيب DMF لتقدير النسبة المولية (M:L “Molar Ratio") و كذلك دراسة الحساسية المغناطيسية لاثبات الصيغة التركيبية المقترحة .
Abstract EN
A new Schiff base, 1,2-bis-[3-(phenyl amino)-5-imino-1,2,4-thiadiazolyl] ethene, was prepared, which was used as ligand to prepare a number of metal complexes of Cr (III), Mn (II), Co (II), Ni (II), Cu (II), Zn (II), Cd (II) and Hg (II).
The products were isolated, studied and characterized by FT.I.R.
spectroscopy, electronic spectroscopy, magnetic susceptibility measurements, conductivity measurements, melting point and elemental analysis (C.H.N.M.).
probable structures of the complexes have been assigned.
American Psychological Association (APA)
al-Jabburi, Mahmud Najm Abd& al-Bayati, Rida Ibrahim& al-Ubaydi, Najat J.. 2006. Synthesis and characterization of some transition metals complexes with 1, 2-bis-[3-(phenyl amino)-5-imino-1, 2, 4 thiadiazolyl] ethene. National Journal of Chemistry،Vol. 2006, no. 22, pp.243-249.
https://search.emarefa.net/detail/BIM-348819
Modern Language Association (MLA)
al-Jabburi, Mahmud Najm Abd…[et al.]. Synthesis and characterization of some transition metals complexes with 1, 2-bis-[3-(phenyl amino)-5-imino-1, 2, 4 thiadiazolyl] ethene. National Journal of Chemistry No. 22 (2006), pp.243-249.
https://search.emarefa.net/detail/BIM-348819
American Medical Association (AMA)
al-Jabburi, Mahmud Najm Abd& al-Bayati, Rida Ibrahim& al-Ubaydi, Najat J.. Synthesis and characterization of some transition metals complexes with 1, 2-bis-[3-(phenyl amino)-5-imino-1, 2, 4 thiadiazolyl] ethene. National Journal of Chemistry. 2006. Vol. 2006, no. 22, pp.243-249.
https://search.emarefa.net/detail/BIM-348819
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 248-249
Record ID
BIM-348819
