Synthesis and characterization of some new complexes with new schiff base type (N2O2) derived from glyoxylic acid and ethylenediamine
Other Title(s)
تحضير و تشخيص بعض المعقدات الجديدة مع قاعدة شف جديدة نوع (N2O2) مشتقة من حامض الكلايوكسيلك مع إثيلين ثنائي أمين
Joint Authors
al-Shammari, Rihab Kazim
Shihab, Jasim Shihab Sultan
Latif, Sajid Mahmud
Source
Ibn al-Haitham Journal for Pure and Applied Science
Issue
Vol. 28, Issue 3 (31 Dec. 2015), pp.72-85, 14 p.
Publisher
University of Baghdad College of Education for Pure Science / Ibn al-Haitham
Publication Date
2015-12-31
Country of Publication
Iraq
No. of Pages
14
Main Subjects
Abstract EN
New tetradentate Schiff base [H2L] namely [2,2 ׳ -(ethane-1,2- diylbis (azan-1-ylylidene) diacetic acid)] was prepared from condensation of ethylenediamine with glyoxylic acid in ethanol as a solvent in presence of drops of 48% HBr .The structure of ligand (H2L) was characterized by,F-IR, U.V-Vis.,1H-,13C-NMR, pectrophotometer,melting point and elemental microanalysis C.H.N.
Metal complexes of the ligand (H2L) in general Molecular formula [M(L)(H2O)2], where M= Co(II), Ni(II), Cu(II), Mn(II) and Hg(II); L=(C6H8N2O4) were synthesized were characterized by, Atomic absorption, F-IR, U.V-Vis.
spectra, molar conductivity and magnetic susceptibility.It was found that all the complexes showed octahedral geometries.And in vitro tests for antibacterial activity showed that most of the prepared compounds display a good activity to (Staphylococcus aureus),(Bacillus cereus ) ,(Escherichia coli) and (Pseudomonas).
American Psychological Association (APA)
al-Shammari, Rihab Kazim& Shihab, Jasim Shihab Sultan& Latif, Sajid Mahmud. 2015. Synthesis and characterization of some new complexes with new schiff base type (N2O2) derived from glyoxylic acid and ethylenediamine. Ibn al-Haitham Journal for Pure and Applied Science،Vol. 28, no. 3, pp.72-85.
https://search.emarefa.net/detail/BIM-679108
Modern Language Association (MLA)
al-Shammari, Rihab Kazim…[et al.]. Synthesis and characterization of some new complexes with new schiff base type (N2O2) derived from glyoxylic acid and ethylenediamine. Ibn al-Haitham Journal for Pure and Applied Science Vol. 28, no. 3 (2015), pp.72-85.
https://search.emarefa.net/detail/BIM-679108
American Medical Association (AMA)
al-Shammari, Rihab Kazim& Shihab, Jasim Shihab Sultan& Latif, Sajid Mahmud. Synthesis and characterization of some new complexes with new schiff base type (N2O2) derived from glyoxylic acid and ethylenediamine. Ibn al-Haitham Journal for Pure and Applied Science. 2015. Vol. 28, no. 3, pp.72-85.
https://search.emarefa.net/detail/BIM-679108
Data Type
Journal Articles
Language
English
Notes
Includes appendix : p. 80-84
Record ID
BIM-679108