Dimeric and tetrameric N…H, C…N and N…N interactions exist in the crystal structure of 8,16-dimethyl-6,7,14,15-tetrahydro-7,15- methanocycloocta [1,2-b:5,6-b’] diquinoline
Joint Authors
Bishop, Roger
al-Shahatit, Sulhi Faysal
al-Ghazzawi, Nawwash Mamduh
Source
Issue
Vol. 6, Issue 2 (30 Jun. 2011), pp.139-151, 13 p.
Publisher
Yarmouk University Deanship of Research and Graduate Studies
Publication Date
2011-06-30
Country of Publication
Jordan
No. of Pages
13
Main Subjects
Topics
Abstract EN
Substituted Diquinoline 3 was synthesized by means of Friedländer condensation.
Series of crystallization experiments were performed and solvent free crystals of diquinoline 3 of X-ray quality were obtained from methanol.
Compound 3 crystallized in the centrosymmetric space group P4 (2) / n of the tetragonal system with unit cell parameters of : a = 11.5536 (7) Å, b = 11.5536 (7) Å, c = 13.1057 (16) Å, with α = 90°, β = 90°, and γ = 90°.
Centrosymmetric tetramer as well as other different supramolecular motifs were observed and analysed in terms of supramolecular chemistry and crystal engineering.
The observed intermolecular interactions were compared to those reported previously for 6 and 7.
American Psychological Association (APA)
al-Shahatit, Sulhi Faysal& al-Ghazzawi, Nawwash Mamduh& Bishop, Roger. 2011. Dimeric and tetrameric N…H, C…N and N…N interactions exist in the crystal structure of 8,16-dimethyl-6,7,14,15-tetrahydro-7,15- methanocycloocta [1,2-b:5,6-b’] diquinoline. Jordan Journal of Chemistry،Vol. 6, no. 2, pp.139-151.
https://search.emarefa.net/detail/BIM-264439
Modern Language Association (MLA)
al-Shahatit, Sulhi Faysal…[et al.]. Dimeric and tetrameric N…H, C…N and N…N interactions exist in the crystal structure of 8,16-dimethyl-6,7,14,15-tetrahydro-7,15- methanocycloocta [1,2-b:5,6-b’] diquinoline. Jordan Journal of Chemistry Vol. 6, no. 2 (Jun. 2011), pp.139-151.
https://search.emarefa.net/detail/BIM-264439
American Medical Association (AMA)
al-Shahatit, Sulhi Faysal& al-Ghazzawi, Nawwash Mamduh& Bishop, Roger. Dimeric and tetrameric N…H, C…N and N…N interactions exist in the crystal structure of 8,16-dimethyl-6,7,14,15-tetrahydro-7,15- methanocycloocta [1,2-b:5,6-b’] diquinoline. Jordan Journal of Chemistry. 2011. Vol. 6, no. 2, pp.139-151.
https://search.emarefa.net/detail/BIM-264439
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 150-151
Record ID
BIM-264439
