Tetraethyl Orthosilicate Coated Hydroxyapatite Powders for Lead Ions Removal from Aqueous Solutions

الملخص EN

The goal of this study was to synthetize and characterize a porous material based on tetraethyl orthosilicate (TEOS) coated hydroxyapatite (HApTh) after removal experiments of Pb2+ ions from aqueous solutions.

In order to study the morphology and composition, the samples obtained after removal experiments of Pb2+ ions from aqueous solution with the initial Pb2+ ion concentrations of the aqueous solutions were 0.1 g·L−1 (HApTh-50) and 0.9 g·L−1 (HApTh-450) have been investigated by scanning electron microscopy (SEM) equipped with an energy dispersive X-ray spectrometer (EDS), Fourier transform infrared spectroscopy (FTIR), and transmission electron microscopy (TEM).

Removal experiments of Pb2+ ions were carried out in aqueous solutions with controlled concentration of Pb2+.

After the removal experiment of Pb2+ ions from solutions, porous hydroxyapatite nanoparticles were transformed into HApTh-50 and HApTh-450 due to the adsorption of Pb2+ ions followed by a cation exchange reaction.

The obtained results show that the porous HApTh nanopowders could be used for Pb2+ ions removal from aqueous solutions.