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Improvements in Drill-Core Headspace Gas Analysis for Samples from Microbially Active Depths
المؤلفون المشاركون
Miyakawa, Kazuya
Okumura, Fumiaki
المصدر
العدد
المجلد 2018، العدد 2018 (31 ديسمبر/كانون الأول 2018)، ص ص. 1-11، 11ص.
الناشر
Hindawi Publishing Corporation
تاريخ النشر
2018-10-01
دولة النشر
مصر
عدد الصفحات
11
التخصصات الرئيسية
الملخص EN
The IsoJar™ container is widely used in headspace gas analysis for gases adsorbed on cuttings or bore cores from oil and gas fields.
However, large variations in the carbon isotopic ratios of CH4 and CO2 are often reported, especially for data obtained from depths of <1000 m.
The IsoJar™ method leaves air in the headspace that allows microbial oxidation of CH4 to CO2, meaning that isotopic fractionation occurs during storage.
This study employed the IsoJar™ method to investigate the causes of differences in δ13C data reported by previous studies in the Horonobe area of Japan.
It was found that after 80 d storage, δ13CCO2 values decreased by ~2‰, while δ13CCH4 values increased by >30‰, whereas samples analyzed within a week of collection showed no such fluctuations.
The conventional amount of microbial suppressant (~0.5 ml of 10% benzalkonium chloride (BKC) solution) is insufficient to suppress microbial activity if groundwater is used as filling water.
The significant variations in carbon isotopic compositions previously reported were caused by microbial methane oxidation after sampling and contamination by groundwater from different depths.
To avoid these problems, we recommend the following: (1) if long-term sample storage is necessary, >10 ml of 10% BKC solution should be added or >0.3% BKC concentration is required to suppress microbial activity; (2) analyses should be performed within one week of sampling; and (3) for CO2 analyses, it is important that samples are not contaminated by groundwater from different depths.
نمط استشهاد جمعية علماء النفس الأمريكية (APA)
Miyakawa, Kazuya& Okumura, Fumiaki. 2018. Improvements in Drill-Core Headspace Gas Analysis for Samples from Microbially Active Depths. Geofluids،Vol. 2018, no. 2018, pp.1-11.
https://search.emarefa.net/detail/BIM-1157325
نمط استشهاد الجمعية الأمريكية للغات الحديثة (MLA)
Miyakawa, Kazuya& Okumura, Fumiaki. Improvements in Drill-Core Headspace Gas Analysis for Samples from Microbially Active Depths. Geofluids No. 2018 (2018), pp.1-11.
https://search.emarefa.net/detail/BIM-1157325
نمط استشهاد الجمعية الطبية الأمريكية (AMA)
Miyakawa, Kazuya& Okumura, Fumiaki. Improvements in Drill-Core Headspace Gas Analysis for Samples from Microbially Active Depths. Geofluids. 2018. Vol. 2018, no. 2018, pp.1-11.
https://search.emarefa.net/detail/BIM-1157325
نوع البيانات
مقالات
لغة النص
الإنجليزية
الملاحظات
Includes bibliographical references
رقم السجل
BIM-1157325
قاعدة معامل التأثير والاستشهادات المرجعية العربي "ارسيف Arcif"
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