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UHPLCMS-MS Analysis of Six Neonicotinoids in Honey by Modified QuEChERS : Method Development, Validation, and Uncertainty Measurement
المؤلفون المشاركون
Morabito, Giovanni
Traulo, Pasqualino
Pantò, Valentina
Sabatino, Leonardo
Chiappara, Elena
Gagliano, Giacomo
Scordino, Monica
Proietto Galeano, Michele
المصدر
International Journal of Food Science
العدد
المجلد 2013، العدد 2013 (31 ديسمبر/كانون الأول 2013)، ص ص. 1-7، 7ص.
الناشر
Hindawi Publishing Corporation
تاريخ النشر
2013-03-31
دولة النشر
مصر
عدد الصفحات
7
التخصصات الرئيسية
العلوم الهندسية و تكنولوجيا المعلومات
الملخص EN
Rapid and reliable multiresidue analytical methods were developed and validated for the determination of 6 neonicotinoids pesticides (acetamiprid, clothianidin, imidacloprid, nitenpyram, thiacloprid, and thiamethoxam) in honey.
A modified QuEChERS method has allowed a very rapid and efficient single-step extraction, while the detection was performed by UHPLC/MS-MS.
The recovery studies were carried out by spiking the samples at two concentration levels (10 and 40 μg/kg).
The methods were subjected to a thorough validation procedure.
The mean recovery was in the range of 75 to 114% with repeatability below 20%.
The limits of detection were below 2.5 μg/kg, while the limits of quantification did not exceed 4.0 μg/kg.
The total uncertainty was evaluated taking the main independent uncertainty sources under consideration.
The expanded uncertainty did not exceed 49% for the 10 μg/kg concentration level and was in the range of 16–19% for the 40 μg/kg fortification level.
نمط استشهاد جمعية علماء النفس الأمريكية (APA)
Proietto Galeano, Michele& Scordino, Monica& Sabatino, Leonardo& Pantò, Valentina& Morabito, Giovanni& Chiappara, Elena…[et al.]. 2013. UHPLCMS-MS Analysis of Six Neonicotinoids in Honey by Modified QuEChERS : Method Development, Validation, and Uncertainty Measurement. International Journal of Food Science،Vol. 2013, no. 2013, pp.1-7.
https://search.emarefa.net/detail/BIM-504431
نمط استشهاد الجمعية الأمريكية للغات الحديثة (MLA)
Proietto Galeano, Michele…[et al.]. UHPLCMS-MS Analysis of Six Neonicotinoids in Honey by Modified QuEChERS : Method Development, Validation, and Uncertainty Measurement. International Journal of Food Science No. 2013 (2013), pp.1-7.
https://search.emarefa.net/detail/BIM-504431
نمط استشهاد الجمعية الطبية الأمريكية (AMA)
Proietto Galeano, Michele& Scordino, Monica& Sabatino, Leonardo& Pantò, Valentina& Morabito, Giovanni& Chiappara, Elena…[et al.]. UHPLCMS-MS Analysis of Six Neonicotinoids in Honey by Modified QuEChERS : Method Development, Validation, and Uncertainty Measurement. International Journal of Food Science. 2013. Vol. 2013, no. 2013, pp.1-7.
https://search.emarefa.net/detail/BIM-504431
نوع البيانات
مقالات
لغة النص
الإنجليزية
الملاحظات
Includes bibliographical references
رقم السجل
BIM-504431
قاعدة معامل التأثير والاستشهادات المرجعية العربي "ارسيف Arcif"
أضخم قاعدة بيانات عربية للاستشهادات المرجعية للمجلات العلمية المحكمة الصادرة في العالم العربي
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