Morphological and Structural Studies of Titanate and Titania Nanostructured Materials Obtained after Heat Treatments of Hydrothermally Produced Layered Titanate

المؤلفون المشاركون

Sreekantan, Srimala
Razali, Mohd Hasmizam
Mohd Noor, Ahmad-Fauzi
Mohamed, Abdul Rahman

المصدر

Journal of Nanomaterials

العدد

المجلد 2012، العدد 2012 (31 ديسمبر/كانون الأول 2012)، ص ص. 1-10، 10ص.

الناشر

Hindawi Publishing Corporation

تاريخ النشر

2012-11-05

دولة النشر

مصر

عدد الصفحات

10

التخصصات الرئيسية

الكيمياء
هندسة مدنية

الملخص EN

Different types of titanate and titania nanostructured materials have been successfully synthesised and characterized using field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), X-ray diffraction (XRD) and raman spectroscopy.

Elemental analysis was determined by energy dispersive X-ray spectroscopy (EDX) analyzer while thermogravimetric-differential scanning calorimetry (TG-DSC) was used to determine thermal stability.

In this study, we found that nanotubes were formed during the washing treatment stage with HCl and distilled water.

When the pH of the washing solution was 12, sodium titanate nanotubes were obtained, while when the pH of the washing solution was 7, hydrogen titanate nanotubes were obtained.

Sodium titanate nanotubes were thermally stable up to 500°C; however, at 700°C, the nanotubes structure transform to solid nanorods.

Meanwhile, hydrogen titanate nanotubes decomposed to produce titania nanotubes after heat treatment at 300°C for 2 hours.

At 500°C, the tubular structure broke to small segments due to destruction of the nanotube.

Further heat treatment at 700°C, led to the destruction and collapse of the nanotubes structure produce titania nanoparticles.

نمط استشهاد جمعية علماء النفس الأمريكية (APA)

Razali, Mohd Hasmizam& Mohd Noor, Ahmad-Fauzi& Mohamed, Abdul Rahman& Sreekantan, Srimala. 2012. Morphological and Structural Studies of Titanate and Titania Nanostructured Materials Obtained after Heat Treatments of Hydrothermally Produced Layered Titanate. Journal of Nanomaterials،Vol. 2012, no. 2012, pp.1-10.
https://search.emarefa.net/detail/BIM-998682

نمط استشهاد الجمعية الأمريكية للغات الحديثة (MLA)

Razali, Mohd Hasmizam…[et al.]. Morphological and Structural Studies of Titanate and Titania Nanostructured Materials Obtained after Heat Treatments of Hydrothermally Produced Layered Titanate. Journal of Nanomaterials No. 2012 (2012), pp.1-10.
https://search.emarefa.net/detail/BIM-998682

نمط استشهاد الجمعية الطبية الأمريكية (AMA)

Razali, Mohd Hasmizam& Mohd Noor, Ahmad-Fauzi& Mohamed, Abdul Rahman& Sreekantan, Srimala. Morphological and Structural Studies of Titanate and Titania Nanostructured Materials Obtained after Heat Treatments of Hydrothermally Produced Layered Titanate. Journal of Nanomaterials. 2012. Vol. 2012, no. 2012, pp.1-10.
https://search.emarefa.net/detail/BIM-998682

نوع البيانات

مقالات

لغة النص

الإنجليزية

الملاحظات

Includes bibliographical references

رقم السجل

BIM-998682