Synthesis characterization of some new heterocyclic compounds containing1, 3-oxazepine ring
Other Title(s)
تحضير وتشخيص بعض المركبات الغير المتجانسة الجديدة المحتوية على حلقة 3,1-اوكسازبي
Joint Authors
Abd al-Wahid, Jawdat Hilmi
Muhammad, Aveen Khayr Allah
Source
Issue
Vol. 11, Issue 3 (30 Sep. 2016), pp.237-247, 11 p.
Publisher
Kirkuk University College of Science
Publication Date
2016-09-30
Country of Publication
Iraq
No. of Pages
11
Main Subjects
Abstract EN
In this work a series of 1, 3-oxazepine derivatives have been synthesized throughout two steps.
First step synthesis of imines derivatives (A1-A7) via the condensation reaction of 4-hydroxy benzaldehyde with different substituted amines by using catalytic amount of glacial acetic acid, while the second step involves reactions of the prepared imines (A1-A7) via maleic anhydride by [2+5] cycloaddition in dry benzene and refluxing it to produce 1, 3 - oxazepine - 4, 7 - dione derivatives (A1m-A7m) respectively.
The prepared compounds were characterized by C.H.N.S micro analysis, some physical properties and spectral methods (IR , H1-NMR).
American Psychological Association (APA)
Abd al-Wahid, Jawdat Hilmi& Hamid, Iyad Sadi& Muhammad, Aveen Khayr Allah. 2016. Synthesis characterization of some new heterocyclic compounds containing1, 3-oxazepine ring. Kirkuk Journal of Science،Vol. 11, no. 3, pp.237-247.
https://search.emarefa.net/detail/BIM-944874
Modern Language Association (MLA)
Hamid, Iyad Sadi…[et al.]. Synthesis characterization of some new heterocyclic compounds containing1, 3-oxazepine ring. Kirkuk Journal of Science Vol. 11, no. 3 (Sep. 2016), pp.237-247.
https://search.emarefa.net/detail/BIM-944874
American Medical Association (AMA)
Abd al-Wahid, Jawdat Hilmi& Hamid, Iyad Sadi& Muhammad, Aveen Khayr Allah. Synthesis characterization of some new heterocyclic compounds containing1, 3-oxazepine ring. Kirkuk Journal of Science. 2016. Vol. 11, no. 3, pp.237-247.
https://search.emarefa.net/detail/BIM-944874
Data Type
Journal Articles
Language
English
Notes
Record ID
BIM-944874