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Determination of Ivermectin in Medicated Feeds by Liquid Chromatography with Fluorescence Detection
Joint Authors
Pietruk, Konrad
Jedziniak, Piotr
Source
Issue
Vol. 2013, Issue 2013 (31 Dec. 2013), pp.1-5, 5 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2013-12-19
Country of Publication
Egypt
No. of Pages
5
Main Subjects
Medicine
Information Technology and Computer Science
Abstract EN
A labour- and time-effective analytical procedure for determination of ivermectin in medicated feed at recommended level of 2.0 mg kg−1 has been developed and validated.
The analyte was extracted from grinded feed samples with acetonitrile and derivatisated with N-methylimidazole and trifluoracetic anhydride.
The fluorescent derivatives were analysed by liquid chromatography method using C8 column.
The isocratic conditions using acetonitrile, methanol, water, and tetrahydrofuran were applied.
Fluorescence detection was performed at 365 nm (excitation) and 475 nm (emission) wavelengths.
The total analysis time was 10 min.
The validation results of the method (within-laboratory reproducibility 4.0% CV, mean recovery 100.1%) confirm the appropriate precision and accuracy of the developed method.
American Psychological Association (APA)
Pietruk, Konrad& Jedziniak, Piotr. 2013. Determination of Ivermectin in Medicated Feeds by Liquid Chromatography with Fluorescence Detection. The Scientific World Journal،Vol. 2013, no. 2013, pp.1-5.
https://search.emarefa.net/detail/BIM-1032818
Modern Language Association (MLA)
Pietruk, Konrad& Jedziniak, Piotr. Determination of Ivermectin in Medicated Feeds by Liquid Chromatography with Fluorescence Detection. The Scientific World Journal No. 2013 (2013), pp.1-5.
https://search.emarefa.net/detail/BIM-1032818
American Medical Association (AMA)
Pietruk, Konrad& Jedziniak, Piotr. Determination of Ivermectin in Medicated Feeds by Liquid Chromatography with Fluorescence Detection. The Scientific World Journal. 2013. Vol. 2013, no. 2013, pp.1-5.
https://search.emarefa.net/detail/BIM-1032818
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1032818