![](/images/graphics-bg.png)
Determination of Decabrominated Diphenyl Ether in Soils by Soxhlet Extraction and High Performance Liquid Chromatography
Joint Authors
Tao, Xue-Qin
Yang, Xing-Jian
Lin, Zhao-Ying
Zou, Meng-Yao
Dang, Zhi
Lu, Gui-Ning
Zhang, Fang-Li
Source
Issue
Vol. 2013, Issue 2013 (31 Dec. 2013), pp.1-6, 6 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2013-11-05
Country of Publication
Egypt
No. of Pages
6
Main Subjects
Medicine
Information Technology and Computer Science
Abstract EN
This study described the development of a method based on soxhlet extraction combining high performance liquid chromatography (soxhlet-HPLC) for the accurate detection of BDE-209 in soils.
The solvent effect of working standard solutions in HPLC was discussed.
Results showed that 1 : 1 of methanol and acetone was the optimal condition which could totally dissolve the BDE-209 in environmental samples and avoid the decrease of the peak area and the peak deformation difference of BDE-209 in HPLC.
The preliminary experiment was conducted on the configured grassland (1 μg/g) to validate the method feasibility.
The method produced reliable reproducibility, simulated soils (n=4) RSD 1.0%, and was further verified by the analysis e-waste contaminated soils, RSD range 5.9–11.4%.
The contamination level of BDE-209 in burning site was consistent with the previous study of Longtang town but lower than Guiyu town, and higher concentration of BDE-209 in paddy field mainly resulted from the long-standing disassembling area nearby.
This accurate and fast method was successfully developed to extract and analyze BDE-209 in soil samples, showing its potential use for replacing GC to determinate BDE-209 in soil samples.
American Psychological Association (APA)
Yang, Xing-Jian& Dang, Zhi& Zhang, Fang-Li& Lin, Zhao-Ying& Zou, Meng-Yao& Tao, Xue-Qin…[et al.]. 2013. Determination of Decabrominated Diphenyl Ether in Soils by Soxhlet Extraction and High Performance Liquid Chromatography. The Scientific World Journal،Vol. 2013, no. 2013, pp.1-6.
https://search.emarefa.net/detail/BIM-1033362
Modern Language Association (MLA)
Yang, Xing-Jian…[et al.]. Determination of Decabrominated Diphenyl Ether in Soils by Soxhlet Extraction and High Performance Liquid Chromatography. The Scientific World Journal No. 2013 (2013), pp.1-6.
https://search.emarefa.net/detail/BIM-1033362
American Medical Association (AMA)
Yang, Xing-Jian& Dang, Zhi& Zhang, Fang-Li& Lin, Zhao-Ying& Zou, Meng-Yao& Tao, Xue-Qin…[et al.]. Determination of Decabrominated Diphenyl Ether in Soils by Soxhlet Extraction and High Performance Liquid Chromatography. The Scientific World Journal. 2013. Vol. 2013, no. 2013, pp.1-6.
https://search.emarefa.net/detail/BIM-1033362
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1033362