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Determination of Norfloxacin and Ciprofloxacin in Chicken Meat Based on Matrix Solid-Phase Dispersion Extraction and Capillary Zone Electrophoresis
Joint Authors
Zhao, Shihao
Zhao, Hongru
Zhu, Hai
Li, Chengyao
Lu, Xinli
Bi, Siyuan
Source
Issue
Vol. 2014, Issue 2014 (31 Dec. 2014), pp.1-5, 5 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2014-05-07
Country of Publication
Egypt
No. of Pages
5
Main Subjects
Abstract EN
This study describes an effective matrix solid-phase dispersion (MSPD) extraction method for determining norfloxacin (NOR) and ciprofloxacin (CIP) in chicken meat by capillary zone electrophoresis (CZE).
The optimum conditions for separating NOR and CIP were as follows: 60 cm×75 μm i.d.
capillary, 40 mmol L−1 borate buffer solution (pH 8.5), separation voltage at 16 kV, and detection wavelength at 280 nm.
Before CZE determination, the chicken meat samples were purified and enriched by using an MSPD extraction step with a preconditioned C18 cartridge and by eluting the compound with 3.0 mL of acetonitrile.
A good linear fit curve with the concentration range of 0.10 μg g−1 to 500 μg g−1 for NOR and CIP was obtained, with regression coefficients of 0.9994 and 0.9986, respectively.
The limits of detection of NOR and CIP were 0.04 and 0.03 μg g−1, respectively.
The proposed method was successfully applied to determine NOR and CIP in chicken meat.
American Psychological Association (APA)
Zhao, Shihao& Zhao, Hongru& Zhu, Hai& Li, Chengyao& Lu, Xinli& Bi, Siyuan. 2014. Determination of Norfloxacin and Ciprofloxacin in Chicken Meat Based on Matrix Solid-Phase Dispersion Extraction and Capillary Zone Electrophoresis. Journal of Chemistry،Vol. 2014, no. 2014, pp.1-5.
https://search.emarefa.net/detail/BIM-1040031
Modern Language Association (MLA)
Zhao, Shihao…[et al.]. Determination of Norfloxacin and Ciprofloxacin in Chicken Meat Based on Matrix Solid-Phase Dispersion Extraction and Capillary Zone Electrophoresis. Journal of Chemistry No. 2014 (2014), pp.1-5.
https://search.emarefa.net/detail/BIM-1040031
American Medical Association (AMA)
Zhao, Shihao& Zhao, Hongru& Zhu, Hai& Li, Chengyao& Lu, Xinli& Bi, Siyuan. Determination of Norfloxacin and Ciprofloxacin in Chicken Meat Based on Matrix Solid-Phase Dispersion Extraction and Capillary Zone Electrophoresis. Journal of Chemistry. 2014. Vol. 2014, no. 2014, pp.1-5.
https://search.emarefa.net/detail/BIM-1040031
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1040031