Analysis of Self-Adhesive Resin Cement Microshear Bond Strength on Leucite-Reinforced Glass-Ceramic withwithout Pure Silane Primer or Universal Adhesive Surface Treatment

Abstract EN

Objective.

To evaluate the microshear bond strength (μSBS) of self-adhesive resin (SA) cement on leucite-reinforced glass-ceramic using silane or universal adhesive.

Materials and Methods.

Ceramic blocks were etched with 9.5% hydrofluoric acid and divided into three groups (n=16): (1) negative control (NC) without treatment; (2) Single Bond Universal (SBU); (3) RelyX Ceramic Primer as positive control (PC).

RelyX Unicem resin cement was light-cured, and μSBS was evaluated with/without thermocycling.

The μSBS was analyzed using one-way analysis of variance.

The fractured surfaces were examined using stereomicroscopy and scanning electron microscopy (SEM).

Results.

Without thermocycling, μSBS was highest for PC (30.50 MPa ± 3.40), followed by SBU (27.33 MPa ± 2.81) and NC (20.18 MPa ± 2.01) (P<0.05).

Thermocycling significantly reduced μSBS in SBU (22.49 MPa ± 4.11) (P<0.05), but not in NC (20.68 MPa ± 4.60) and PC (28.77 MPa ± 3.52) (P>0.05).

PC and NC predominantly fractured by cohesive failure within the ceramic and mixed failure, respectively.

Conclusion.

SBU treatment improves μSBS between SA cement and glass ceramics, but to a lower value than PC, and the improvement is eradicated by thermocycling.

NC exhibited the lowest μSBS, which remained unchanged after thermocycling.