Separation of Berberine Hydrochloride and Tetrahydropalmatine and Their Quantitative Analysis with Thin Layer Chromatography Involved with Ionic Liquids
Joint Authors
Lu, Jing
Yao, Shun
Ma, Hong-yan
Zhang, Wei
Ma, Zhi-guo
Source
Journal of Analytical Methods in Chemistry
Issue
Vol. 2015, Issue 2015 (31 Dec. 2015), pp.1-7, 7 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2015-11-01
Country of Publication
Egypt
No. of Pages
7
Main Subjects
Abstract EN
[BMIM]OH was used in mobile and stationary phase of thin layer chromatography (TLC) to analyze berberine hydrochloride and tetrahydropalmatine for the first time.
Supported imidazole ionic liquid with hydroxide ion on silica gel (SiO2·Im+·OH−) was synthesized through simple procedure and characterized by Fourier transform infrared spectroscopy (FT-IR), elemental analysis, and scanning electron microscope (SEM).
Moreover, on the plates prepared by SiO2·Im+·OH−, the contents of the above alkaloids in the Chinese patent medicine (CPM) of “Stomacheasy” capsule were successfully determined by TLC scanner.
The key conditions and chromatographic behaviors were also investigated in detail.
According to similar ways, ionic liquids (ILs) also can be used in other planar chromatographies in two modes.
This study is expected to be helpful in expanding the application of IL and its bonded silica gel in TLC separation field.
American Psychological Association (APA)
Lu, Jing& Ma, Hong-yan& Zhang, Wei& Ma, Zhi-guo& Yao, Shun. 2015. Separation of Berberine Hydrochloride and Tetrahydropalmatine and Their Quantitative Analysis with Thin Layer Chromatography Involved with Ionic Liquids. Journal of Analytical Methods in Chemistry،Vol. 2015, no. 2015, pp.1-7.
https://search.emarefa.net/detail/BIM-1067222
Modern Language Association (MLA)
Lu, Jing…[et al.]. Separation of Berberine Hydrochloride and Tetrahydropalmatine and Their Quantitative Analysis with Thin Layer Chromatography Involved with Ionic Liquids. Journal of Analytical Methods in Chemistry No. 2015 (2015), pp.1-7.
https://search.emarefa.net/detail/BIM-1067222
American Medical Association (AMA)
Lu, Jing& Ma, Hong-yan& Zhang, Wei& Ma, Zhi-guo& Yao, Shun. Separation of Berberine Hydrochloride and Tetrahydropalmatine and Their Quantitative Analysis with Thin Layer Chromatography Involved with Ionic Liquids. Journal of Analytical Methods in Chemistry. 2015. Vol. 2015, no. 2015, pp.1-7.
https://search.emarefa.net/detail/BIM-1067222
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1067222