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Comparison of the Usefulness of SPE Cartridges for the Determination of β-Blockers and β-Agonists (Basic Drugs) in Environmental Aqueous Samples
Joint Authors
Caban, Magda
Stepnowski, Piotr
Kwiatkowski, Marek
Maszkowska, Joanna
Wagil, Marta
Kumirska, Jolanta
Source
Issue
Vol. 2015, Issue 2015 (31 Dec. 2015), pp.1-9, 9 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2015-03-26
Country of Publication
Egypt
No. of Pages
9
Main Subjects
Abstract EN
Even though the methodology used for the determination of β-blockers and β-agonists in environmental samples is based mainly on solid-phase extraction (SPE) and gas chromatography or liquid chromatography with mass spectrometric detection, the available literature data on the applied SPE procedures is rather sparse.
In this paper such comparison is presented.
Moreover, the usefulness of the eight SPE cartridges for the determination of five β-blockers (acebutolol, atenolol, metoprolol, nadolol, and propranolol) and two β-agonists (salbutamol and terbutaline) in environmental aqueous samples using GC techniques is tested.
Among them, three (the trifunction sorbent Strata Screen C, the copolymers LiChrolut EN, and the functionalized copolymer Isolute ENV+) were used for the first time for this purpose.
It was confirmed that polystyrene-divinylbenzene-N-vinylpyrrolidone copolymers (PS-DVB-VP, Strata-X, and Oasis HLB cartridges) have a better potential than a cation-exchange sorbent for the extraction of the target drugs from environmental water samples.
However, it should be stressed out that the direct application of the tested SPE conditions for the analysis of real environmental water samples is not possible, and such parameters, like volume of loading sample, appropriate solvents for washing and elution steps, and so forth, must be optimized again in order to achieve satisfactory recovery values for the target compounds.
American Psychological Association (APA)
Caban, Magda& Stepnowski, Piotr& Kwiatkowski, Marek& Maszkowska, Joanna& Wagil, Marta& Kumirska, Jolanta. 2015. Comparison of the Usefulness of SPE Cartridges for the Determination of β-Blockers and β-Agonists (Basic Drugs) in Environmental Aqueous Samples. Journal of Chemistry،Vol. 2015, no. 2015, pp.1-9.
https://search.emarefa.net/detail/BIM-1067338
Modern Language Association (MLA)
Caban, Magda…[et al.]. Comparison of the Usefulness of SPE Cartridges for the Determination of β-Blockers and β-Agonists (Basic Drugs) in Environmental Aqueous Samples. Journal of Chemistry No. 2015 (2015), pp.1-9.
https://search.emarefa.net/detail/BIM-1067338
American Medical Association (AMA)
Caban, Magda& Stepnowski, Piotr& Kwiatkowski, Marek& Maszkowska, Joanna& Wagil, Marta& Kumirska, Jolanta. Comparison of the Usefulness of SPE Cartridges for the Determination of β-Blockers and β-Agonists (Basic Drugs) in Environmental Aqueous Samples. Journal of Chemistry. 2015. Vol. 2015, no. 2015, pp.1-9.
https://search.emarefa.net/detail/BIM-1067338
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1067338