Synthesis and Crystal Structure of N-Dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine
Joint Authors
Ye, Fei
Gao, Shuang
Qu, Hai-Tao
Fu, Ying
Source
Issue
Vol. 2015, Issue 2015 (31 Dec. 2015), pp.1-5, 5 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2015-08-06
Country of Publication
Egypt
No. of Pages
5
Main Subjects
Abstract EN
A new compound, N-dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine, was synthesized and characterized.
The crystal structure of the title compound (C11H10Cl3NO2, M r = 294.55 ) has been determined by single-crystal X-ray diffraction.
The crystal belongs to monoclinic, space group P 2 1 / c , with a = 6.7619 ( 14 ) , b = 24.866 ( 5 ) , c = 9.737 ( 3 ) Å, α = 90.00 , β = 130.982 ( 18 ) , γ = 90.00 ° , V = 1235.9 ( 5 ) Å3, Z = 4 , D x = 1.583 Mg/cm3, λ ( Mo K a ) = 0.71073 Å, F ( 000 ) = 600 , μ = 0.729 mm−1, R = 0.0476 , and w R = 0.1274 for 2217 reflections with I > 2 σ ( I ) .
American Psychological Association (APA)
Gao, Shuang& Qu, Hai-Tao& Ye, Fei& Fu, Ying. 2015. Synthesis and Crystal Structure of N-Dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine. Journal of Chemistry،Vol. 2015, no. 2015, pp.1-5.
https://search.emarefa.net/detail/BIM-1067385
Modern Language Association (MLA)
Gao, Shuang…[et al.]. Synthesis and Crystal Structure of N-Dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine. Journal of Chemistry No. 2015 (2015), pp.1-5.
https://search.emarefa.net/detail/BIM-1067385
American Medical Association (AMA)
Gao, Shuang& Qu, Hai-Tao& Ye, Fei& Fu, Ying. Synthesis and Crystal Structure of N-Dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine. Journal of Chemistry. 2015. Vol. 2015, no. 2015, pp.1-5.
https://search.emarefa.net/detail/BIM-1067385
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1067385