Synthesis and Crystal Structure of N-Dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine

Joint Authors

Ye, Fei
Gao, Shuang
Qu, Hai-Tao
Fu, Ying

Source

Journal of Chemistry

Issue

Vol. 2015, Issue 2015 (31 Dec. 2015), pp.1-5, 5 p.

Publisher

Hindawi Publishing Corporation

Publication Date

2015-08-06

Country of Publication

Egypt

No. of Pages

5

Main Subjects

Chemistry

Abstract EN

A new compound, N-dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine, was synthesized and characterized.

The crystal structure of the title compound (C11H10Cl3NO2, M r = 294.55 ) has been determined by single-crystal X-ray diffraction.

The crystal belongs to monoclinic, space group P 2 1 / c , with a = 6.7619 ( 14 ) , b = 24.866 ( 5 ) , c = 9.737 ( 3 ) Å, α = 90.00 , β = 130.982 ( 18 ) , γ = 90.00 ° , V = 1235.9 ( 5 ) Å3, Z = 4 , D x = 1.583 Mg/cm3, λ ( Mo K a ) = 0.71073 Å, F ( 000 ) = 600 , μ = 0.729 mm−1, R = 0.0476 , and w R = 0.1274 for 2217 reflections with I > 2 σ ( I ) .

American Psychological Association (APA)

Gao, Shuang& Qu, Hai-Tao& Ye, Fei& Fu, Ying. 2015. Synthesis and Crystal Structure of N-Dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine. Journal of Chemistry،Vol. 2015, no. 2015, pp.1-5.
https://search.emarefa.net/detail/BIM-1067385

Modern Language Association (MLA)

Gao, Shuang…[et al.]. Synthesis and Crystal Structure of N-Dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine. Journal of Chemistry No. 2015 (2015), pp.1-5.
https://search.emarefa.net/detail/BIM-1067385

American Medical Association (AMA)

Gao, Shuang& Qu, Hai-Tao& Ye, Fei& Fu, Ying. Synthesis and Crystal Structure of N-Dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine. Journal of Chemistry. 2015. Vol. 2015, no. 2015, pp.1-5.
https://search.emarefa.net/detail/BIM-1067385

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references

Record ID

BIM-1067385