![](/images/graphics-bg.png)
Synthesis, Optical Characterization, and Thermal Decomposition of Complexes Based on Biuret Ligand
Joint Authors
Zhong, Guo-Qing
Wang, Mei-Ling
Chen, Ling
Source
International Journal of Optics
Issue
Vol. 2016, Issue 2016 (31 Dec. 2016), pp.1-8, 8 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2016-02-25
Country of Publication
Egypt
No. of Pages
8
Main Subjects
Abstract EN
Four complexes were synthesized in methanol solution using nickel acetate or nickel chloride, manganese acetate, manganese chloride, and biuret as raw materials.
The complexes were characterized by elemental analyses, UV, FTIR, Raman spectra, X-ray powder diffraction, and thermogravimetric analysis.
The compositions of the complexes were [Ni(bi)2(H2O)2](Ac)2·H2O (1), [Ni(bi)2Cl2] (2), [Mn(bi)2(Ac)2]·1.5H2O (3), and [Mn(bi)2Cl2] (4) (bi = NH2CONHCONH2), respectively.
In the complexes, every metal ion was coordinated by oxygen atoms or chlorine ions and even both.
The nickel and manganese ions were all hexacoordinated.
The thermal decomposition processes of the complexes under air included the loss of water molecule, the pyrolysis of ligands, and the decomposition of inorganic salts, and the final residues were nickel oxide and manganese oxide, respectively.
American Psychological Association (APA)
Wang, Mei-Ling& Zhong, Guo-Qing& Chen, Ling. 2016. Synthesis, Optical Characterization, and Thermal Decomposition of Complexes Based on Biuret Ligand. International Journal of Optics،Vol. 2016, no. 2016, pp.1-8.
https://search.emarefa.net/detail/BIM-1106371
Modern Language Association (MLA)
Wang, Mei-Ling…[et al.]. Synthesis, Optical Characterization, and Thermal Decomposition of Complexes Based on Biuret Ligand. International Journal of Optics No. 2016 (2016), pp.1-8.
https://search.emarefa.net/detail/BIM-1106371
American Medical Association (AMA)
Wang, Mei-Ling& Zhong, Guo-Qing& Chen, Ling. Synthesis, Optical Characterization, and Thermal Decomposition of Complexes Based on Biuret Ligand. International Journal of Optics. 2016. Vol. 2016, no. 2016, pp.1-8.
https://search.emarefa.net/detail/BIM-1106371
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1106371