Application of Multivariable Analysis and FTIR-ATR Spectroscopy to the Prediction of Properties in Campeche Honey
Joint Authors
Anguebes, Francisco
Pat, Lucio
Ali, Bassam
Guerrero, Armando
Córdova, Atl V.
Abatal, Mohamed
Garduza, José P.
Source
Journal of Analytical Methods in Chemistry
Issue
Vol. 2016, Issue 2016 (31 Dec. 2016), pp.1-14, 14 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2016-12-14
Country of Publication
Egypt
No. of Pages
14
Main Subjects
Abstract EN
Attenuated total reflectance-Fourier transform infrared spectrometry and chemometrics model was used for determination of physicochemical properties (pH, redox potential, free acidity, electrical conductivity, moisture, total soluble solids (TSS), ash, and HMF) in honey samples.
The reference values of 189 honey samples of different botanical origin were determined using Association Official Analytical Chemists, (AOAC), 1990; Codex Alimentarius, 2001, International Honey Commission, 2002, methods.
Multivariate calibration models were built using partial least squares (PLS) for the measurands studied.
The developed models were validated using cross-validation and external validation; several statistical parameters were obtained to determine the robustness of the calibration models: (PCs) optimum number of components principal, (SECV) standard error of cross-validation, ( R 2 c a l ) coefficient of determination of cross-validation, (SEP) standard error of validation, and ( R 2 v a l ) coefficient of determination for external validation and coefficient of variation (CV).
The prediction accuracy for pH, redox potential, electrical conductivity, moisture, TSS, and ash was good, while for free acidity and HMF it was poor.
The results demonstrate that attenuated total reflectance-Fourier transform infrared spectrometry is a valuable, rapid, and nondestructive tool for the quantification of physicochemical properties of honey.
American Psychological Association (APA)
Anguebes, Francisco& Pat, Lucio& Ali, Bassam& Guerrero, Armando& Córdova, Atl V.& Abatal, Mohamed…[et al.]. 2016. Application of Multivariable Analysis and FTIR-ATR Spectroscopy to the Prediction of Properties in Campeche Honey. Journal of Analytical Methods in Chemistry،Vol. 2016, no. 2016, pp.1-14.
https://search.emarefa.net/detail/BIM-1107338
Modern Language Association (MLA)
Anguebes, Francisco…[et al.]. Application of Multivariable Analysis and FTIR-ATR Spectroscopy to the Prediction of Properties in Campeche Honey. Journal of Analytical Methods in Chemistry No. 2016 (2016), pp.1-14.
https://search.emarefa.net/detail/BIM-1107338
American Medical Association (AMA)
Anguebes, Francisco& Pat, Lucio& Ali, Bassam& Guerrero, Armando& Córdova, Atl V.& Abatal, Mohamed…[et al.]. Application of Multivariable Analysis and FTIR-ATR Spectroscopy to the Prediction of Properties in Campeche Honey. Journal of Analytical Methods in Chemistry. 2016. Vol. 2016, no. 2016, pp.1-14.
https://search.emarefa.net/detail/BIM-1107338
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1107338