Synthesis and Characterization of Molecular Imprinting Polymer Microspheres of Piperine: Extraction of Piperine from Spiked Urine
Joint Authors
Roland, Rachel Marcella
Bhawani, Showkat A.
Source
Journal of Analytical Methods in Chemistry
Issue
Vol. 2016, Issue 2016 (31 Dec. 2016), pp.1-6, 6 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2016-11-27
Country of Publication
Egypt
No. of Pages
6
Main Subjects
Abstract EN
Molecularly imprinted polymer (MIP) microspheres for Piperine were synthesized by precipitation polymerization with a noncovalent approach.
In this research Piperine was used as a template, acrylic acid as a functional monomer, ethylene glycol dimethacrylate as a cross-linker, and 2,2′-azobisisobutyronitrile (AIBN) as an initiator and acetonitrile as a solvent.
The imprinted and nonimprinted polymer particles were characterized by using Fourier transform infrared spectroscopy (FT-IR) and Scanning Electron Microscopy (SEM).
The synthesized polymer particles were further evaluated for their rebinding efficiency by batch binding assay.
The highly selected imprinted polymer for Piperine was MIP 3 with a composition (molar ratio) of 0.5 : 3 : 8, template : monomer : cross-linker, respectively.
The MIP 3 exhibits highest binding capacity (84.94%) as compared to other imprinted and nonimprinted polymers.
The extraction efficiency of highly selected imprinted polymer of Piperine from spiked urine was above 80%.
American Psychological Association (APA)
Roland, Rachel Marcella& Bhawani, Showkat A.. 2016. Synthesis and Characterization of Molecular Imprinting Polymer Microspheres of Piperine: Extraction of Piperine from Spiked Urine. Journal of Analytical Methods in Chemistry،Vol. 2016, no. 2016, pp.1-6.
https://search.emarefa.net/detail/BIM-1107340
Modern Language Association (MLA)
Roland, Rachel Marcella& Bhawani, Showkat A.. Synthesis and Characterization of Molecular Imprinting Polymer Microspheres of Piperine: Extraction of Piperine from Spiked Urine. Journal of Analytical Methods in Chemistry No. 2016 (2016), pp.1-6.
https://search.emarefa.net/detail/BIM-1107340
American Medical Association (AMA)
Roland, Rachel Marcella& Bhawani, Showkat A.. Synthesis and Characterization of Molecular Imprinting Polymer Microspheres of Piperine: Extraction of Piperine from Spiked Urine. Journal of Analytical Methods in Chemistry. 2016. Vol. 2016, no. 2016, pp.1-6.
https://search.emarefa.net/detail/BIM-1107340
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1107340