Synthesis and characterization of new 1,2,4- triazole derivatives form 2-naphthol
Joint Authors
Abd al-Razzaq, Nur
Awdah, Sadun Abd Allah
Atiyyah, Abbas Jasim
Source
Journal of Babylon University : Journal of Applied and Pure Sciences
Issue
Vol. 26, Issue 6 (30 Jun. 2018), pp.234-252, 19 p.
Publisher
Publication Date
2018-06-30
Country of Publication
Iraq
No. of Pages
19
Main Subjects
Abstract EN
In this work 1,2,4-triazole derivatives were synthesized from [4-(2-hydroxy naphthyl)diazenyl]benzoic acid [N1] then converted to [4-(2-hydroxy naphthyl)diazenyl] benzoate [N2] which reacted with thiosemicarbazide and then cyclization by using sodium hydroxide.
Then different alkyl halides like (methyl iodide, allyl chloride, proprgyl chloride and benzyl chloride) were added to[4-(2-hydroxy naphthyl)diazenyl]-4H-1,2,4-triazole-3-thiol [N4] that led to alkylation of thiol to afforded compounds [N5] – [N8].
These compounds were characterized by the following techniques: FT-IR, and 1H , 13C NMR spectroscopies, and elemental analysis C.H.N.S.
The physical properties of prepared compounds were studied.-
American Psychological Association (APA)
Abd al-Razzaq, Nur& Awdah, Sadun Abd Allah& Atiyyah, Abbas Jasim. 2018. Synthesis and characterization of new 1,2,4- triazole derivatives form 2-naphthol. Journal of Babylon University : Journal of Applied and Pure Sciences،Vol. 26, no. 6, pp.234-252.
https://search.emarefa.net/detail/BIM-1120404
Modern Language Association (MLA)
Abd al-Razzaq, Nur…[et al.]. Synthesis and characterization of new 1,2,4- triazole derivatives form 2-naphthol. Journal of Babylon University : Journal of Applied and Pure Sciences Vol. 26, no. 6 (2018), pp.234-252.
https://search.emarefa.net/detail/BIM-1120404
American Medical Association (AMA)
Abd al-Razzaq, Nur& Awdah, Sadun Abd Allah& Atiyyah, Abbas Jasim. Synthesis and characterization of new 1,2,4- triazole derivatives form 2-naphthol. Journal of Babylon University : Journal of Applied and Pure Sciences. 2018. Vol. 26, no. 6, pp.234-252.
https://search.emarefa.net/detail/BIM-1120404
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 252
Record ID
BIM-1120404