Synthesis of Ti2SnC under Optimized Experimental Parameters of Pressureless Spark Plasma Sintering Assisted by Al Addition
Joint Authors
Zhang, Jianfeng
Lu, Chen
Wang, Yue
Wang, Xiaofan
Source
Advances in Materials Science and Engineering
Issue
Vol. 2018, Issue 2018 (31 Dec. 2018), pp.1-9, 9 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2018-03-27
Country of Publication
Egypt
No. of Pages
9
Abstract EN
As an effective and novel rapid sintering technology with the advantages of fast heating speed and short sintering time, SPS has been applied to the research and development of various materials.
After sintering at 1325°C, Ti5Sn3 and Sn occurred as impurities accompanying the synthesis of Ti2SnC with a raw powder mixture of Ti/Sn/C = 2/1/1 (molar ratio).
But by addition of 0.2 molar Al, and further optimization of sintering parameters at 1400°C for 10 min, almost fully pure Ti2SnC was obtained with a clear layered microstructure.
The reaction mechanism analysis suggests that this beneficial effect of Al could be attributed to the suppression of decomposition of Ti2SnC by formation of Ti2SnxAl1−xC solid solution at a high sintering temperature.
The present study reports a novel route to synthesize Ti2SnC by PL-SPS with a self-designed graphite die, and Al was also proposed as a sintering aid to remove impurities.
American Psychological Association (APA)
Lu, Chen& Wang, Yue& Wang, Xiaofan& Zhang, Jianfeng. 2018. Synthesis of Ti2SnC under Optimized Experimental Parameters of Pressureless Spark Plasma Sintering Assisted by Al Addition. Advances in Materials Science and Engineering،Vol. 2018, no. 2018, pp.1-9.
https://search.emarefa.net/detail/BIM-1122522
Modern Language Association (MLA)
Lu, Chen…[et al.]. Synthesis of Ti2SnC under Optimized Experimental Parameters of Pressureless Spark Plasma Sintering Assisted by Al Addition. Advances in Materials Science and Engineering No. 2018 (2018), pp.1-9.
https://search.emarefa.net/detail/BIM-1122522
American Medical Association (AMA)
Lu, Chen& Wang, Yue& Wang, Xiaofan& Zhang, Jianfeng. Synthesis of Ti2SnC under Optimized Experimental Parameters of Pressureless Spark Plasma Sintering Assisted by Al Addition. Advances in Materials Science and Engineering. 2018. Vol. 2018, no. 2018, pp.1-9.
https://search.emarefa.net/detail/BIM-1122522
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1122522