Optimization of Resolving Power, Fragmentation, and Mass Calibration in an Orbitrap Spectrometer for Analysis of 24 Pesticide Metabolites in Urine

Joint Authors

Dualde, Pablo
Coscollà, Clara
Yusà, Vicent
Pastor, Agustin

Source

International Journal of Analytical Chemistry

Issue

Vol. 2019, Issue 2019 (31 Dec. 2019), pp.1-12, 12 p.

Publisher

Hindawi Publishing Corporation

Publication Date

2019-04-17

Country of Publication

Egypt

No. of Pages

12

Main Subjects

Chemistry
Science

Abstract EN

Mass spectrometer parameters such as Resolving Power, type of fragmentation, and mass calibration mode were optimized in the analysis of 24 pesticide metabolites in human urine using Ultra-High Pressure Liquid Chromatography coupled to Orbitrap High-Resolution Mass Spectrometer (UHPLC-HRMS).

The best results were achieved with a Resolving Power of 25,000 FWHM and by applying Collision Induced Dissociation fragmentation mode (40 eV).

American Psychological Association (APA)

Dualde, Pablo& Coscollà, Clara& Pastor, Agustin& Yusà, Vicent. 2019. Optimization of Resolving Power, Fragmentation, and Mass Calibration in an Orbitrap Spectrometer for Analysis of 24 Pesticide Metabolites in Urine. International Journal of Analytical Chemistry،Vol. 2019, no. 2019, pp.1-12.
https://search.emarefa.net/detail/BIM-1155845

Modern Language Association (MLA)

Dualde, Pablo…[et al.]. Optimization of Resolving Power, Fragmentation, and Mass Calibration in an Orbitrap Spectrometer for Analysis of 24 Pesticide Metabolites in Urine. International Journal of Analytical Chemistry No. 2019 (2019), pp.1-12.
https://search.emarefa.net/detail/BIM-1155845

American Medical Association (AMA)

Dualde, Pablo& Coscollà, Clara& Pastor, Agustin& Yusà, Vicent. Optimization of Resolving Power, Fragmentation, and Mass Calibration in an Orbitrap Spectrometer for Analysis of 24 Pesticide Metabolites in Urine. International Journal of Analytical Chemistry. 2019. Vol. 2019, no. 2019, pp.1-12.
https://search.emarefa.net/detail/BIM-1155845

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references

Record ID

BIM-1155845