A Green and Efficient Method for the Preconcentration and Determination of Gallic Acid, Bergenin, Quercitrin, and Embelin from Ardisia japonica Using Nononic Surfactant Genapol X-080 as the Extraction Solvent
Joint Authors
Chang, Yanxu
Li, Jin
An, Mingrui
Tan, Zhijing
Bai, Yun
Chen, Ying
Du, Kunze
Source
International Journal of Analytical Chemistry
Issue
Vol. 2018, Issue 2018 (31 Dec. 2018), pp.1-10, 10 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2018-02-01
Country of Publication
Egypt
No. of Pages
10
Main Subjects
Abstract EN
A simple cloud point preconcentration method was developed and validated for the determination of gallic acid, bergenin, quercitrin, and embelin in Ardisia japonica by high-performance liquid chromatography (HPLC) using ultrasonic assisted micellar extraction.
Nonionic surfactant Genapol X-080 was selected as the extraction solvent.
The effects of various experimental conditions such as the type and concentration of surfactant and salt, temperature, and solution pH on the extraction of these components were studied to optimize the conditions of Ardisia japonica.
The solution was incubated in a thermostatic water bath at 60°C for 10 min, and 35% NaH2PO4 (w/v) was added to the solution to promote the phase separation and increase the preconcentration factor.
The intraday and interday precision (RSD) were both below 5.0% and the limits of detection (LOD) for the analytes were between 10 and 20 ng·mL−1.
The proposed method provides a simple, efficient, and organic solvent-free method to analyze gallic acid, bergenin, quercitrin, and embelin for the quality control of Ardisia japonica.
American Psychological Association (APA)
Chen, Ying& Du, Kunze& Li, Jin& Bai, Yun& An, Mingrui& Tan, Zhijing…[et al.]. 2018. A Green and Efficient Method for the Preconcentration and Determination of Gallic Acid, Bergenin, Quercitrin, and Embelin from Ardisia japonica Using Nononic Surfactant Genapol X-080 as the Extraction Solvent. International Journal of Analytical Chemistry،Vol. 2018, no. 2018, pp.1-10.
https://search.emarefa.net/detail/BIM-1166299
Modern Language Association (MLA)
Chen, Ying…[et al.]. A Green and Efficient Method for the Preconcentration and Determination of Gallic Acid, Bergenin, Quercitrin, and Embelin from Ardisia japonica Using Nononic Surfactant Genapol X-080 as the Extraction Solvent. International Journal of Analytical Chemistry No. 2018 (2018), pp.1-10.
https://search.emarefa.net/detail/BIM-1166299
American Medical Association (AMA)
Chen, Ying& Du, Kunze& Li, Jin& Bai, Yun& An, Mingrui& Tan, Zhijing…[et al.]. A Green and Efficient Method for the Preconcentration and Determination of Gallic Acid, Bergenin, Quercitrin, and Embelin from Ardisia japonica Using Nononic Surfactant Genapol X-080 as the Extraction Solvent. International Journal of Analytical Chemistry. 2018. Vol. 2018, no. 2018, pp.1-10.
https://search.emarefa.net/detail/BIM-1166299
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1166299