Inter-Laboratory Validation of Method to Determine Residual Enrofloxacin in Chicken Meat
Joint Authors
Chung, Joo Hee
Cho, Kun
Kim, Seongnyeon
Jeon, So Hyeon
Shin, Jeoung Hwa
Lee, Jueun
Ahn, Yun Gyong
Source
International Journal of Analytical Chemistry
Issue
Vol. 2018, Issue 2018 (31 Dec. 2018), pp.1-7, 7 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2018-06-10
Country of Publication
Egypt
No. of Pages
7
Main Subjects
Abstract EN
An inter-laboratory study was performed to evaluate the performance of a method developed for the quantification of enrofloxacin in chicken meat.
Liquid-liquid extraction combined with a clean-up procedure based on solid-phase extraction followed by a liquid chromatography-tandem mass spectrometric method was used by three individual laboratories.
All the investigated results of calibration curves and limits of quantification were within the acceptable range for regulatory testing of enrofloxacin.
The three laboratories received blind a certified reference material to analyze in triplicate and assess using statistical analysis.
From the results, no statistical differences were found between the laboratories in the precision of the method.
Additionally, all the results of the z-score, which is an indication of fixed interval bias criteria for accuracy from the laboratories, fell within the allowable limits (±2σ).
Based on this proficiency testing by inter-laboratory comparisons, the analytical method including the sample preparation step was proven to be applicable.
American Psychological Association (APA)
Chung, Joo Hee& Cho, Kun& Kim, Seongnyeon& Jeon, So Hyeon& Shin, Jeoung Hwa& Lee, Jueun…[et al.]. 2018. Inter-Laboratory Validation of Method to Determine Residual Enrofloxacin in Chicken Meat. International Journal of Analytical Chemistry،Vol. 2018, no. 2018, pp.1-7.
https://search.emarefa.net/detail/BIM-1166446
Modern Language Association (MLA)
Chung, Joo Hee…[et al.]. Inter-Laboratory Validation of Method to Determine Residual Enrofloxacin in Chicken Meat. International Journal of Analytical Chemistry No. 2018 (2018), pp.1-7.
https://search.emarefa.net/detail/BIM-1166446
American Medical Association (AMA)
Chung, Joo Hee& Cho, Kun& Kim, Seongnyeon& Jeon, So Hyeon& Shin, Jeoung Hwa& Lee, Jueun…[et al.]. Inter-Laboratory Validation of Method to Determine Residual Enrofloxacin in Chicken Meat. International Journal of Analytical Chemistry. 2018. Vol. 2018, no. 2018, pp.1-7.
https://search.emarefa.net/detail/BIM-1166446
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1166446