Rapid Screening of Volatile Organic Compounds from Aframomum danielli Seeds Using Headspace Solid Phase Microextraction Coupled to Gas Chromatography Mass Spectrometry
Joint Authors
Madala, N. E.
Dubery, Ian A.
Gbashi, Sefater
Njobeh, Patrick
George, Mosotho J.
Adegoke, Gabriel O.
Source
International Journal of Analytical Chemistry
Issue
Vol. 2018, Issue 2018 (31 Dec. 2018), pp.1-7, 7 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2018-04-19
Country of Publication
Egypt
No. of Pages
7
Main Subjects
Abstract EN
Volatile organic compounds (VOCs) derived from plants have been used in the fragrance industry since time immemorial.
Herein we report on the rapid screening of VOCs from seeds of ripe Aframomum danielli (family, Zingiberaceae) using a polydimethylsiloxane fibre headspace solid phase microextraction coupled to a gas chromatography mass spectrometry (SPME-GC/MS) instrument.
Portions of 0.25, 0.35, and 0.50 g of ground sample were weighed and extraction of volatile organic compounds (VOCs) was achieved using a 100 μm polydimethylsiloxane solid phase microextraction (PDMS SPME) fibre, with the equilibrium time of 40 minutes and extraction temperature of 50°C; the following compounds with their respective relative abundances were obtained as the top ten most abundant and annotated ones using NIST, Wiley, and Fragrances Libraries: eucalyptol (58%); β-pinene (22%); α-pinene (7.5%); α-terpineol (4%), α-terpinyl acetate (2%); α-bergamotene (1%); pinocarveol (0.39%); α-copaene (0.35%); caryophyllene (0.34); and β-bisabolene (0.31%).
These compounds have been reported elsewhere in the literature and listed in the Fragrances Library, incorporated into the Saturn QP2020 GCMS Solution® software used for their analysis.
American Psychological Association (APA)
George, Mosotho J.& Njobeh, Patrick& Gbashi, Sefater& Adegoke, Gabriel O.& Dubery, Ian A.& Madala, N. E.. 2018. Rapid Screening of Volatile Organic Compounds from Aframomum danielli Seeds Using Headspace Solid Phase Microextraction Coupled to Gas Chromatography Mass Spectrometry. International Journal of Analytical Chemistry،Vol. 2018, no. 2018, pp.1-7.
https://search.emarefa.net/detail/BIM-1166537
Modern Language Association (MLA)
George, Mosotho J.…[et al.]. Rapid Screening of Volatile Organic Compounds from Aframomum danielli Seeds Using Headspace Solid Phase Microextraction Coupled to Gas Chromatography Mass Spectrometry. International Journal of Analytical Chemistry No. 2018 (2018), pp.1-7.
https://search.emarefa.net/detail/BIM-1166537
American Medical Association (AMA)
George, Mosotho J.& Njobeh, Patrick& Gbashi, Sefater& Adegoke, Gabriel O.& Dubery, Ian A.& Madala, N. E.. Rapid Screening of Volatile Organic Compounds from Aframomum danielli Seeds Using Headspace Solid Phase Microextraction Coupled to Gas Chromatography Mass Spectrometry. International Journal of Analytical Chemistry. 2018. Vol. 2018, no. 2018, pp.1-7.
https://search.emarefa.net/detail/BIM-1166537
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1166537