Synthesis and characterization of new zinc-phthalocyanine with four dodecenyl-benzoic pendant groups
Joint Authors
Source
Journal of Babylon University : Journal of Applied and Pure Sciences
Issue
Vol. 25, Issue 2 (30 Jun. 2017), pp.486-496, 11 p.
Publisher
Publication Date
2017-06-30
Country of Publication
Iraq
No. of Pages
11
Main Subjects
Abstract EN
Substituted zinc phthalocyanine was synthesized in this study.
The reaction of 4- nitro Phthalonitrile with ZnCl2 in the presence of dimethyl amino ethanol (DMEA) afforded 4,4ʹ,4ʹʹ,4ʹʹʹ- tetranitro zinc phthalocyanine.
This was reacted with 5-amino salicylic acid to yield tetra-(5-amino salicylic acid)zinc phthalocyanine.
After that, dodecenyl succinic anhydride was added on amine group of benzoic rings afforded tetra-( (E)-5-(3-(dodec-1-enyl)-2,5-dioxopyrrolidin-1-yl)-2-hydroxybenzoic acid )zinc phthalocyanine.
The phthalocyanine was separated and washed using different solvents.
The newly synthesized compounds have been characterized by elemental analysis, FT-IR, 1H NMR and UV-Visible spectroscopy techniques.
American Psychological Association (APA)
al-Bahrani, Husayn Ali Muhammad Jafar& Karim, Muhannad Musa. 2017. Synthesis and characterization of new zinc-phthalocyanine with four dodecenyl-benzoic pendant groups. Journal of Babylon University : Journal of Applied and Pure Sciences،Vol. 25, no. 2, pp.486-496.
https://search.emarefa.net/detail/BIM-1169523
Modern Language Association (MLA)
al-Bahrani, Husayn Ali Muhammad Jafar& Karim, Muhannad Musa. Synthesis and characterization of new zinc-phthalocyanine with four dodecenyl-benzoic pendant groups. Journal of Babylon University : Journal of Applied and Pure Sciences Vol. 25, no. 2 (2017), pp.486-496.
https://search.emarefa.net/detail/BIM-1169523
American Medical Association (AMA)
al-Bahrani, Husayn Ali Muhammad Jafar& Karim, Muhannad Musa. Synthesis and characterization of new zinc-phthalocyanine with four dodecenyl-benzoic pendant groups. Journal of Babylon University : Journal of Applied and Pure Sciences. 2017. Vol. 25, no. 2, pp.486-496.
https://search.emarefa.net/detail/BIM-1169523
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 496
Record ID
BIM-1169523