Development of QuEChERS Method for the Determination of Polycyclic Aromatic Hydrocarbons in Smoked Meat Products Using GC-MS from Qatar
Joint Authors
Al-Thaiban, Hussain
Al-Tamimi, Nada
Helaleh, Murad
Source
Journal of Analytical Methods in Chemistry
Issue
Vol. 2018, Issue 2018 (31 Dec. 2018), pp.1-11, 11 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2018-07-18
Country of Publication
Egypt
No. of Pages
11
Main Subjects
Abstract EN
A simple and fast method for the determination of PAHs in smoked meat samples was described.
The QuEChERS (Z-Sep) procedure was used for sample preparation.
Gas chromatograph-mass spectrometer with electron ionization (EI) was used to separate and detect the PAHs.
All 16 common PAHs were analyzed successfully.
Matrix-matched calibration was applied.
Spiked samples were performed at 1 ng/g (n=10) and 10 ng/g (n=10) for two days.
Overall recoveries of PAHs were within 74 to 117%, with RSDs within 1.15 to 37.57% and 1 and 10 ng/g wet weight for first and second day, respectively.
In most of the analyzed smoked meat samples, there were no exceeded levels compared to the maximum levels declared by Commission Regulation (EU) number 835/2011.
The method can be recommended for routine analysis for laboratories having a large number of samples.
American Psychological Association (APA)
Al-Thaiban, Hussain& Al-Tamimi, Nada& Helaleh, Murad. 2018. Development of QuEChERS Method for the Determination of Polycyclic Aromatic Hydrocarbons in Smoked Meat Products Using GC-MS from Qatar. Journal of Analytical Methods in Chemistry،Vol. 2018, no. 2018, pp.1-11.
https://search.emarefa.net/detail/BIM-1176658
Modern Language Association (MLA)
Al-Thaiban, Hussain…[et al.]. Development of QuEChERS Method for the Determination of Polycyclic Aromatic Hydrocarbons in Smoked Meat Products Using GC-MS from Qatar. Journal of Analytical Methods in Chemistry No. 2018 (2018), pp.1-11.
https://search.emarefa.net/detail/BIM-1176658
American Medical Association (AMA)
Al-Thaiban, Hussain& Al-Tamimi, Nada& Helaleh, Murad. Development of QuEChERS Method for the Determination of Polycyclic Aromatic Hydrocarbons in Smoked Meat Products Using GC-MS from Qatar. Journal of Analytical Methods in Chemistry. 2018. Vol. 2018, no. 2018, pp.1-11.
https://search.emarefa.net/detail/BIM-1176658
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1176658