Synthesis and Characterization of PVP-Stabilized Palladium Nanoparticles by XRD, SAXS, SP-ICP-MS, and SEM
Joint Authors
Walbrück, Katharina
Kuellmer, Fabian
Witzleben, Steffen
Guenther, Klaus
Source
Issue
Vol. 2019, Issue 2019 (31 Dec. 2019), pp.1-7, 7 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2019-04-17
Country of Publication
Egypt
No. of Pages
7
Main Subjects
Abstract EN
Due to increased emissions of palladium nanoparticles in recent years, it is important to develop analytical techniques to characterize these particles.
The synthesis of defined and stable particles plays a key role in this process, as there are not many materials commercially available yet which could act as reference materials.
Polyvinylpyrrolidone- (PVP-) stabilized palladium nanoparticles were synthesized through the reduction of palladium chloride by tetraethylene glycol (TEG) in the presence of KOH.
Four different methods were used for particle size analysis of the palladium nanoparticles.
Palladium suspensions were analyzed by scanning electron microscopy (SEM), small angle X-ray scattering (SAXS), single-particle ICP-MS (SP-ICP-MS), and X-ray diffraction (XRD).
Secondary particles between 30 nm and 130 nm were detected in great compliance with SAXS and SP-ICP-MS.
SEM analysis showed that the small particulates tend to form agglomerates.
American Psychological Association (APA)
Walbrück, Katharina& Kuellmer, Fabian& Witzleben, Steffen& Guenther, Klaus. 2019. Synthesis and Characterization of PVP-Stabilized Palladium Nanoparticles by XRD, SAXS, SP-ICP-MS, and SEM. Journal of Nanomaterials،Vol. 2019, no. 2019, pp.1-7.
https://search.emarefa.net/detail/BIM-1182347
Modern Language Association (MLA)
Walbrück, Katharina…[et al.]. Synthesis and Characterization of PVP-Stabilized Palladium Nanoparticles by XRD, SAXS, SP-ICP-MS, and SEM. Journal of Nanomaterials No. 2019 (2019), pp.1-7.
https://search.emarefa.net/detail/BIM-1182347
American Medical Association (AMA)
Walbrück, Katharina& Kuellmer, Fabian& Witzleben, Steffen& Guenther, Klaus. Synthesis and Characterization of PVP-Stabilized Palladium Nanoparticles by XRD, SAXS, SP-ICP-MS, and SEM. Journal of Nanomaterials. 2019. Vol. 2019, no. 2019, pp.1-7.
https://search.emarefa.net/detail/BIM-1182347
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1182347