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Efficient Preparation and Performance Characterization of the HMXF2602 Microspheres by One-Step Granulation Process
Joint Authors
Jia, Xinlei
Zhang, Yuanping
Hou, Conghua
Tan, Yingxin
Wang, Jingyu
Li, Chao
Source
Issue
Vol. 2017, Issue 2017 (31 Dec. 2017), pp.1-7, 7 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2017-12-18
Country of Publication
Egypt
No. of Pages
7
Main Subjects
Abstract EN
A new one-step granulation process for preparing high melting explosive- (HMX-) based PBX was developed.
HMX/F2602 microspheres were successfully prepared by using HMX and F2602 as the main explosive and binder, respectively.
The particle morphology, particle size, crystal structure, thermal stability, and impact sensitivity of the as-prepared HMX/F2602 microspheres were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), laser particle size analyzer, differential scanning calorimetry (DSC), and impact sensitivity test, respectively.
The SEM analysis indicated successful coating of F2602 on the surface of HMX, and the resulting particles are ellipsoidal or spherical with a median particle size of 940 nm; the XRD analysis did not show any change in the crystal structure after the coating and still has β-HNX crystal structure; according to the DSC analysis, HMX/F2602 prepared by the new method has better thermal stability compared to that prepared by the water suspension process.
The impact sensitivity of HMX/F2602 prepared by this one-step granulation process decreased, and its characteristic height H50 increased from 37.62 to 40.13 cm, thus significantly improving the safety performance.
More importantly, this method does not need the freeze-drying process after recrystallization, thus increasing the efficiency by 2 to 3 times.
American Psychological Association (APA)
Hou, Conghua& Jia, Xinlei& Wang, Jingyu& Tan, Yingxin& Zhang, Yuanping& Li, Chao. 2017. Efficient Preparation and Performance Characterization of the HMXF2602 Microspheres by One-Step Granulation Process. Journal of Nanomaterials،Vol. 2017, no. 2017, pp.1-7.
https://search.emarefa.net/detail/BIM-1182909
Modern Language Association (MLA)
Tan, Yingxin…[et al.]. Efficient Preparation and Performance Characterization of the HMXF2602 Microspheres by One-Step Granulation Process. Journal of Nanomaterials No. 2017 (2017), pp.1-7.
https://search.emarefa.net/detail/BIM-1182909
American Medical Association (AMA)
Hou, Conghua& Jia, Xinlei& Wang, Jingyu& Tan, Yingxin& Zhang, Yuanping& Li, Chao. Efficient Preparation and Performance Characterization of the HMXF2602 Microspheres by One-Step Granulation Process. Journal of Nanomaterials. 2017. Vol. 2017, no. 2017, pp.1-7.
https://search.emarefa.net/detail/BIM-1182909
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-1182909