Synthesis and Characterization of High-Purity Ultrafine Platinum Particles by Chemical Refining Method

Joint Authors

Zhao, Panchao
Yi, Wei
Cao, Qigao
Zhang, Bosheng
Chen, Kunkun
Li, Jigang
Yao, Chensiqi

Source

Journal of Nanomaterials

Issue

Vol. 2019, Issue 2019 (31 Dec. 2019), pp.1-8, 8 p.

Publisher

Hindawi Publishing Corporation

Publication Date

2019-03-25

Country of Publication

Egypt

No. of Pages

8

Main Subjects

Chemistry
Civil Engineering

Abstract EN

High-purity ultrafine platinum particles are widely used to fabricate platinum electrode oxygen sensors for automobiles and thick-film platinum resistance temperature elements.

In this study, the near-spherical ultrafine Pt particles of high purity were synthesized by chemical purification, spray-drying, and ignition from crude Pt powder.

Impurities in the initial Pt powder were eliminated by the 001×7 strong acid cation resin exchange column and precipitation treatment.

Near-spherical (NH4)2PtCl6 particles were obtained after spray-drying, and then the microstructure and size of as-synthesized Pt particles were controlled by the ignition process.

The influences of different heating temperatures during ignition treatment on the microstructure and size of Pt particles were investigated.

The purity of as-synthesized Pt particles was higher than 99.999 wt%, and the average size was about 1.12 μm.

The results indicate that high-purity ultrafine Pt particles can be efficiently synthesized by chemical refining.

American Psychological Association (APA)

Zhao, Panchao& Yi, Wei& Cao, Qigao& Zhang, Bosheng& Chen, Kunkun& Li, Jigang…[et al.]. 2019. Synthesis and Characterization of High-Purity Ultrafine Platinum Particles by Chemical Refining Method. Journal of Nanomaterials،Vol. 2019, no. 2019, pp.1-8.
https://search.emarefa.net/detail/BIM-1183209

Modern Language Association (MLA)

Zhao, Panchao…[et al.]. Synthesis and Characterization of High-Purity Ultrafine Platinum Particles by Chemical Refining Method. Journal of Nanomaterials No. 2019 (2019), pp.1-8.
https://search.emarefa.net/detail/BIM-1183209

American Medical Association (AMA)

Zhao, Panchao& Yi, Wei& Cao, Qigao& Zhang, Bosheng& Chen, Kunkun& Li, Jigang…[et al.]. Synthesis and Characterization of High-Purity Ultrafine Platinum Particles by Chemical Refining Method. Journal of Nanomaterials. 2019. Vol. 2019, no. 2019, pp.1-8.
https://search.emarefa.net/detail/BIM-1183209

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references

Record ID

BIM-1183209