Microwave assisted synthesis of 3, 5-diaryl-2-pyrazolines and pyrazoles
Joint Authors
al-Shehry, Hana A.
Korraa, Makarem M.S.
al-Hazimi, Hasan Muhammad Ahmad,
Source
Journal of Saudi Chemical Society
Issue
Vol. 12, Issue 3 (30 Sep. 2008)10 p.
Publisher
Publication Date
2008-09-30
Country of Publication
Saudi Arabia
No. of Pages
10
Main Subjects
Topics
Abstract AR
شيدت 3، 5-ثنائي أريل-2-بيرازولينات 2a-p عن طريق تكثف الشالكونات la-g مع الهيدرازين و مشتقات N-ميثيل و N-فينيل و ذلك بواسطة تقنية التشعيع بالميكروويف.
و قد تم الحصول على هذه البيرازولينات بمردود جيد و في وقت قصير جدا، مقارنة بتلك البارزولينات التي تم تشييدها بطريقة التسخين التقليدية.
و بالمثل، فإن تفاعل مركب 1، 4-ثنائي كربونيل مع الهيدرازينات و الهيدرازيدات بواسطة الميكروويف أدى إلى تكون البيرازولات 3a-h و 4d-d بمردود متوسط.
و قد تم التعرف على كل المركبات المشيدة بالطرق الطيفية المختلفة.
Abstract EN
3, 5-Diaryl-2-pyrazolines 2a-p were synthesized by the condensation of chalcones 1a-g with hydrazine and its N-methyl and N-phenyl derivatives using microwave irradiation.
The pyrazolines were obtained in high yields and in a very short time in comparison to those of 2-pyrazolines achieved by conventional method.
Similarly, the reaction of a 1, 4-dicarbonyl compound with hydrazines and hydrazides under microwave procedure led to the formation of pyrazoles 3a-h and 4a-d in moderate yields.
Structural elucidation of all synthesized compounds was based on the various spectroscopic methods.
American Psychological Association (APA)
al-Shehry, Hana A.& al-Hazimi, Hasan Muhammad Ahmad,& Korraa, Makarem M.S.. 2008. Microwave assisted synthesis of 3, 5-diaryl-2-pyrazolines and pyrazoles. Journal of Saudi Chemical Society،Vol. 12, no. 3.
https://search.emarefa.net/detail/BIM-20808
Modern Language Association (MLA)
al-Shehry, Hana A.…[et al.]. Microwave assisted synthesis of 3, 5-diaryl-2-pyrazolines and pyrazoles. Journal of Saudi Chemical Society Vol. 12, no. 3 (Sep. 2008).
https://search.emarefa.net/detail/BIM-20808
American Medical Association (AMA)
al-Shehry, Hana A.& al-Hazimi, Hasan Muhammad Ahmad,& Korraa, Makarem M.S.. Microwave assisted synthesis of 3, 5-diaryl-2-pyrazolines and pyrazoles. Journal of Saudi Chemical Society. 2008. Vol. 12, no. 3.
https://search.emarefa.net/detail/BIM-20808
Data Type
Journal Articles
Language
English
Notes
includes bibliographical references
Record ID
BIM-20808