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Synthesis and characterization of tolbutamide-molybdenum complex by thermal, spectral and X-ray studies
Joint Authors
Iqbal, S. A.
Jacob, George
Zafrani, Ishaq Abd Allah Ali
Source
Journal of Saudi Chemical Society
Issue
Vol. 14, Issue 4 (31 Dec. 2010), pp.345-350, 6 p.
Publisher
Publication Date
2010-12-31
Country of Publication
Saudi Arabia
No. of Pages
6
Main Subjects
Abstract EN
Synthesis and characterization of molybdenum complex with tolbutamide (an oral antidiabetic drug) have been studied.
The conduct metric titration using monovariation method indicates that complex is non-ionic and of L2M type.
Analytical data agree with the molecular formula (C12H17N203S)2Mo-2H20.
Structure of the complex was assigned as octahedral in which ligand molecules lie horizontally joining the central molybdenum atom and one water molecule, each attached vertically with the metal.
Infra-red spectral studies confirm the coordination of sulphonyl oxygen on one side and enolic oxygen attached from other side with the metal ion.
IRand'HNMR studies support structure II proposed on the basis of analytical data.
Magnetic susceptibility data suggested that the complex is diamagnetic.
Thermal studies support the presence of ligand moieties and coordinated water.
X-ray diffraction data also support the complex formation.
American Psychological Association (APA)
Iqbal, S. A.& Jacob, George& Zafrani, Ishaq Abd Allah Ali. 2010. Synthesis and characterization of tolbutamide-molybdenum complex by thermal, spectral and X-ray studies. Journal of Saudi Chemical Society،Vol. 14, no. 4, pp.345-350.
https://search.emarefa.net/detail/BIM-250289
Modern Language Association (MLA)
Iqbal, S. A.…[et al.]. Synthesis and characterization of tolbutamide-molybdenum complex by thermal, spectral and X-ray studies. Journal of Saudi Chemical Society (Dec. 2010), pp.345-350.
https://search.emarefa.net/detail/BIM-250289
American Medical Association (AMA)
Iqbal, S. A.& Jacob, George& Zafrani, Ishaq Abd Allah Ali. Synthesis and characterization of tolbutamide-molybdenum complex by thermal, spectral and X-ray studies. Journal of Saudi Chemical Society. 2010. Vol. 14, no. 4, pp.345-350.
https://search.emarefa.net/detail/BIM-250289
Data Type
Journal Articles
Language
English
Notes
44
Record ID
BIM-250289