Synthesis and characterization of some new 1, 3-oxazepine derivatives
Other Title(s)
تحضير و تشخيص بعض مشتقات 1، 3-أوكسازبين الجديدة
Author
Source
Ibn al-Haitham Journal for Pure and Applied Science
Issue
Vol. 24, Issue 1 (31 Mar. 2011)9 p.
Publisher
University of Baghdad College of Education for Pure Science / Ibn al-Haitham
Publication Date
2011-03-31
Country of Publication
Iraq
No. of Pages
9
Main Subjects
Abstract AR
في هذه الدراسة حضرت قواعد شف من تكاثف ن–ثنائي مثيل امينو بنزالديهايد، و 4- مثيل بنزالديهيايد مع امين حلقي أولي [ن-(مثيل هايدرازينيل].
فوعلت قواعد شف المحضرة مع انهدريد الماليك و انهدريد الفثاليك إعطاء مركبات 3،1-أوكسازبين [S5, S6, S7,S8] بنسبة منتوج جيدة.
شخصت المركبات المحضرة بوساطة درجة الانصهار، و صفائح الكروموتوكرافية الرقيقة، وطيف الأشعة تحت الحمراء FT.IR، و طيف الرنين النووي المغناطيسي 1H-NMR.
Abstract EN
In this study, Schiff's bases [S3, S4] were synthesized by condensation of N,N-dimethyl amino benzaldehyde with primary aromatic amine[N-(hydrazinyl methyl) benzamide].
These Schiff's bases were found to react with maleic anhydride and phthalic anhydride to give 1,3-Oxazepine[S5,S6,S7,S8] in good yields.
The structures conferred by m.
p ,T.L.C.,FT.IR and 1H-NMR (of some of them.
American Psychological Association (APA)
Saud, Shayma Abd. 2011. Synthesis and characterization of some new 1, 3-oxazepine derivatives. Ibn al-Haitham Journal for Pure and Applied Science،Vol. 24, no. 1.
https://search.emarefa.net/detail/BIM-286852
Modern Language Association (MLA)
Saud, Shayma Abd. Synthesis and characterization of some new 1, 3-oxazepine derivatives. Ibn al-Haitham Journal for Pure and Applied Science Vol. 24, no. 1 (2011).
https://search.emarefa.net/detail/BIM-286852
American Medical Association (AMA)
Saud, Shayma Abd. Synthesis and characterization of some new 1, 3-oxazepine derivatives. Ibn al-Haitham Journal for Pure and Applied Science. 2011. Vol. 24, no. 1.
https://search.emarefa.net/detail/BIM-286852
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-286852