Synthesis and characterization of some new 1, 3-oxazepine derivatives

Other Title(s)

تحضير و تشخيص بعض مشتقات 1، 3-أوكسازبين الجديدة

Author

Saud, Shayma Abd

Source

Ibn al-Haitham Journal for Pure and Applied Science

Issue

Vol. 24, Issue 1 (31 Mar. 2011)9 p.

Publisher

University of Baghdad College of Education for Pure Science / Ibn al-Haitham

Publication Date

2011-03-31

Country of Publication

Iraq

No. of Pages

9

Main Subjects

Chemistry

Abstract AR

في هذه الدراسة حضرت قواعد شف من تكاثف ن–ثنائي مثيل امينو بنزالديهايد، و 4- مثيل بنزالديهيايد مع امين حلقي أولي [ن-(مثيل هايدرازينيل].

فوعلت قواعد شف المحضرة مع انهدريد الماليك و انهدريد الفثاليك إعطاء مركبات 3،1-أوكسازبين [S5, S6, S7,S8] بنسبة منتوج جيدة.

شخصت المركبات المحضرة بوساطة درجة الانصهار، و صفائح الكروموتوكرافية الرقيقة، وطيف الأشعة تحت الحمراء FT.IR، و طيف الرنين النووي المغناطيسي 1H-NMR.

Abstract EN

In this study, Schiff's bases [S3, S4] were synthesized by condensation of N,N-dimethyl amino benzaldehyde with primary aromatic amine[N-(hydrazinyl methyl) benzamide].

These Schiff's bases were found to react with maleic anhydride and phthalic anhydride to give 1,3-Oxazepine[S5,S6,S7,S8] in good yields.

The structures conferred by m.

p ,T.L.C.,FT.IR and 1H-NMR (of some of them.

American Psychological Association (APA)

Saud, Shayma Abd. 2011. Synthesis and characterization of some new 1, 3-oxazepine derivatives. Ibn al-Haitham Journal for Pure and Applied Science،Vol. 24, no. 1.
https://search.emarefa.net/detail/BIM-286852

Modern Language Association (MLA)

Saud, Shayma Abd. Synthesis and characterization of some new 1, 3-oxazepine derivatives. Ibn al-Haitham Journal for Pure and Applied Science Vol. 24, no. 1 (2011).
https://search.emarefa.net/detail/BIM-286852

American Medical Association (AMA)

Saud, Shayma Abd. Synthesis and characterization of some new 1, 3-oxazepine derivatives. Ibn al-Haitham Journal for Pure and Applied Science. 2011. Vol. 24, no. 1.
https://search.emarefa.net/detail/BIM-286852

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references

Record ID

BIM-286852