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Spectrofluorimetric method for the determination of glibenclamide in pharmaceutical formulations
Other Title(s)
طريقة تقدير الكليبنكلامايد بطريقة الفلورة في الخلطات الصيدلانية
Joint Authors
Khalaf, Karim Dimah
Hasan, Perween Ahmad
Source
Issue
Vol. 9, Issue 2 (31 Dec. 2012), pp.296-301, 6 p.
Publisher
University of Baghdad College of Science for Women
Publication Date
2012-12-31
Country of Publication
Iraq
No. of Pages
6
Main Subjects
Pharmacy, Health & Medical Sciences
Topics
Abstract AR
يعرض البحث طريقة لتقدير مركب الكليبنكلامايد في الخلطات الصيدلانية باستخدام ظاهرة الفلورة.
تعتمد هذه الطريقة على إذابة المركب في الكحول المطلق و قياس شدة فلورته الطبيعية عند طول موجي مقداره 354 نانوميتر بعد إثارته عند الطول الموجي 302 نانوميتر.
يشير الرسم البياني لشدة الفلورة مقابل التركيز بأن قانوني بير ينطبق ضمن مدى التركيز من 1.4 إلى 10 مايكرو غرام/ ملليلتر و انحراف قياسي مقداره 0.0614.
Abstract EN
A sensitive spectrofluorimetric method for the determination of glibenclamide in its tablet formulations has been proposed.
The method is based on the dissolving of glibenclamide in absolute ethanol and measuring the native fluorescence at 354 nm after excitation at 302 nm.
Beers law is obeyed in the concentration of 1.4 to 10 μg.ml-1 of glibenclamide with a limit of detection (LD) of 0.067 μg.
ml -1 and a standard deviation of 0.614.
The range percent recoveries (N = 3) is 94–103.
American Psychological Association (APA)
Khalaf, Karim Dimah& Hasan, Perween Ahmad. 2012. Spectrofluorimetric method for the determination of glibenclamide in pharmaceutical formulations. Baghdad Science Journal،Vol. 9, no. 2, pp.296-301.
https://search.emarefa.net/detail/BIM-303819
Modern Language Association (MLA)
Khalaf, Karim Dimah& Hasan, Perween Ahmad. Spectrofluorimetric method for the determination of glibenclamide in pharmaceutical formulations. Baghdad Science Journal Vol. 9, no. 2 (Dec. 2012), pp.296-301.
https://search.emarefa.net/detail/BIM-303819
American Medical Association (AMA)
Khalaf, Karim Dimah& Hasan, Perween Ahmad. Spectrofluorimetric method for the determination of glibenclamide in pharmaceutical formulations. Baghdad Science Journal. 2012. Vol. 9, no. 2, pp.296-301.
https://search.emarefa.net/detail/BIM-303819
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 299-300
Record ID
BIM-303819