A New approach to the synthesis of2- Isopropoxyphenyl N- methyl carbamate
Author
Source
Iraqi National Journal of Chemistry
Issue
Vol. 2012, Issue 46 (30 Jun. 2012), pp.240-249, 10 p.
Publisher
University of Babylon College of Sciences
Publication Date
2012-06-30
Country of Publication
Iraq
No. of Pages
10
Main Subjects
Abstract AR
ايزوبروبوكسي فنيل-N- مثيل كاربميت (و هي المادة الفعالة لمبيد البايكون) حضر عبر طريقة جديدة و ذلك من خلال تفاعل الكاتيكول مع 2-كلوروبروبان في وسط قاعدي لنحصل على المركب ايزوبروبوكسي فينول و عند مفاعلته مع المركب كلوريد الكاربونيل حصلنا على 2-ايزوبروبوكسي فنيل كلورو فورميت.
حيث تم مفاعلة الأخير مع مثيل أمين بوسط قاعدي من ثلاثي مثيل أمين ليعطي الناتج بكمية جيدة و نسبة عالية.
Abstract EN
2-IsopropoxyphenylN-methyl carbomate (5) which are the active ingredient of the trade name baygonpesticides had been prepared by reacting equal mole of catechol with 2- chloropropanein a basic medium followed by treatment with carbonyl chloride in dry toluene at zeroCo,togive,2-isopropoxyphenylchloro formate (4).
Reaction of the later with methyl amine in presence of base afforded the required product (5).
The structure of the product was diagnosed by comparing it is physical properties and spectral data with the litertures(1)
American Psychological Association (APA)
Husayn, Salim H.. 2012. A New approach to the synthesis of2- Isopropoxyphenyl N- methyl carbamate. Iraqi National Journal of Chemistry،Vol. 2012, no. 46, pp.240-249.
https://search.emarefa.net/detail/BIM-316310
Modern Language Association (MLA)
Husayn, Salim H.. A New approach to the synthesis of2- Isopropoxyphenyl N- methyl carbamate. Iraqi National Journal of Chemistry No. 46 (Jun. 2012), pp.240-249.
https://search.emarefa.net/detail/BIM-316310
American Medical Association (AMA)
Husayn, Salim H.. A New approach to the synthesis of2- Isopropoxyphenyl N- methyl carbamate. Iraqi National Journal of Chemistry. 2012. Vol. 2012, no. 46, pp.240-249.
https://search.emarefa.net/detail/BIM-316310
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 248-249
Record ID
BIM-316310