A New approach to the synthesis of2- Isopropoxyphenyl N- methyl carbamate

Author

Husayn, Salim H.

Source

Iraqi National Journal of Chemistry

Issue

Vol. 2012, Issue 46 (30 Jun. 2012), pp.240-249, 10 p.

Publisher

University of Babylon College of Sciences

Publication Date

2012-06-30

Country of Publication

Iraq

No. of Pages

10

Main Subjects

Chemistry

Abstract AR

ايزوبروبوكسي فنيل-N- مثيل كاربميت (و هي المادة الفعالة لمبيد البايكون) حضر عبر طريقة جديدة و ذلك من خلال تفاعل الكاتيكول مع 2-كلوروبروبان في وسط قاعدي لنحصل على المركب ايزوبروبوكسي فينول و عند مفاعلته مع المركب كلوريد الكاربونيل حصلنا على 2-ايزوبروبوكسي فنيل كلورو فورميت.

حيث تم مفاعلة الأخير مع مثيل أمين بوسط قاعدي من ثلاثي مثيل أمين ليعطي الناتج بكمية جيدة و نسبة عالية.

Abstract EN

2-IsopropoxyphenylN-methyl carbomate (5) which are the active ingredient of the trade name baygonpesticides had been prepared by reacting equal mole of catechol with 2- chloropropanein a basic medium followed by treatment with carbonyl chloride in dry toluene at zeroCo,togive,2-isopropoxyphenylchloro formate (4).

Reaction of the later with methyl amine in presence of base afforded the required product (5).

The structure of the product was diagnosed by comparing it is physical properties and spectral data with the litertures(1)

American Psychological Association (APA)

Husayn, Salim H.. 2012. A New approach to the synthesis of2- Isopropoxyphenyl N- methyl carbamate. Iraqi National Journal of Chemistry،Vol. 2012, no. 46, pp.240-249.
https://search.emarefa.net/detail/BIM-316310

Modern Language Association (MLA)

Husayn, Salim H.. A New approach to the synthesis of2- Isopropoxyphenyl N- methyl carbamate. Iraqi National Journal of Chemistry No. 46 (Jun. 2012), pp.240-249.
https://search.emarefa.net/detail/BIM-316310

American Medical Association (AMA)

Husayn, Salim H.. A New approach to the synthesis of2- Isopropoxyphenyl N- methyl carbamate. Iraqi National Journal of Chemistry. 2012. Vol. 2012, no. 46, pp.240-249.
https://search.emarefa.net/detail/BIM-316310

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references : p. 248-249

Record ID

BIM-316310