Preparing of barium titanate using chemical method and studying of its structural properties
Other Title(s)
تحضير مادة باريوم تيتانيت بالطريقة الكيميائية و دراسة خصائصها التركيبية
Joint Authors
Ismail, Mukhlis Mawlud
Khalaf, Abd al-Karim Z.
Hilal, Rawa A.
Salman, Adi N.
Ramadan, Thawra F.
Source
Engineering and Technology Journal
Issue
Vol. 30, Issue 19 (31 Dec. 2012), pp.3362-3370, 9 p.
Publisher
Publication Date
2012-12-31
Country of Publication
Iraq
No. of Pages
9
Main Subjects
Abstract AR
تم تحضير باريوم تيتانيت أحادي التبلور باستخدام (TiCl) و (BaCl²) بطريقة حامض الاوكزاليك.
أظهرت نتائج الدراسة بأن مادة الباريوم تيتانيت ذات طور رباعي و ذلك عن طريق تحليلات ال(XRD) و (HRTEM) .
و كذلك من خلال حرق المسحوق الناتج إلى درجة 750 ظهر المسحوق بشكله النقي.
الصور المأخوذة لمسحوق الباريوم تيتانيت (TEM) أظهرت كروية الشكل عند حرقه إلى درجة 230، بينما تغيرت أشكاله إلى أصابع توأمية، و أشكال شجيرية و جنينية عند حرقه عند درجة 530 و 750 على التوالي.
Abstract EN
Single crystalline BaTiO3 (BT) was prepared using TiCl4, BaCl2 and oxalic acid.
The structure of the prepared nanocrystalline BT powders were a tetragonal perovskite according to XRD and HRTEM analysis.
Annealing powder to 750oC show that pure BT phase was formed according to XRD, TG, and FTIR spectroscopy.
The TEM images of the prepared powder reveal spherical morphology of BT, while a finger twin, dendritic and embryo shape are observed of BT powder calcined at 230, 530, and 750oC respectively.
SAED and HRTEM images showed a high crystalline BT powder and a single crystalline BT respectively.
American Psychological Association (APA)
Ismail, Mukhlis Mawlud& Khalaf, Abd al-Karim Z.& Hilal, Rawa A.& Salman, Adi N.& Ramadan, Thawra F.. 2012. Preparing of barium titanate using chemical method and studying of its structural properties. Engineering and Technology Journal،Vol. 30, no. 19, pp.3362-3370.
https://search.emarefa.net/detail/BIM-320639
Modern Language Association (MLA)
Ismail, Mukhlis Mawlud…[et al.]. Preparing of barium titanate using chemical method and studying of its structural properties. Engineering and Technology Journal Vol. 30, no. 19 (2012), pp.3362-3370.
https://search.emarefa.net/detail/BIM-320639
American Medical Association (AMA)
Ismail, Mukhlis Mawlud& Khalaf, Abd al-Karim Z.& Hilal, Rawa A.& Salman, Adi N.& Ramadan, Thawra F.. Preparing of barium titanate using chemical method and studying of its structural properties. Engineering and Technology Journal. 2012. Vol. 30, no. 19, pp.3362-3370.
https://search.emarefa.net/detail/BIM-320639
Data Type
Journal Articles
Language
English
Notes
Includes appendices : p. 3366-3370
Record ID
BIM-320639
