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Synthesis and characterization of palladium (II) and platinum (II) complexes with quinazoline and thiolate derivatives
Other Title(s)
تحضير و تشخيص عدد من معقدات البلاديوم و البلاتين مع مشتقات الكوينازولين و الثايوليت
Author
Source
Issue
Vol. 19, Issue 2 (31 Aug. 2008), pp.42-47, 6 p.
Publisher
University of Mosul College of Science
Publication Date
2008-08-31
Country of Publication
Iraq
No. of Pages
6
Main Subjects
Abstract AR
تم تحضير عدد من معقدات pd + 2 و pt + 2 مع -2مثيل -3- أمينوكينوزولين -4- أون (L1) و -2مثيل -3- هيدروكسي كوينازولين -4-أون (L2) بالتفاعل المباشر بين Na2PdCl4 أو K2PtCl مع الليكاندات.
كذلك تم تحضير المعقدات التي تمتلك الصيغة العامة ] M(L) (SC6H4.P-Me) 2 خلال تفاعل الاستبدال النيكلوفيلي.
تم تشخيص المعتقدات المحضرة بوساطة أطياف UV / Vis , IR و القياسات المغناطيسية و قياسات التوصل الكهربائي.
تبين من نتائج الطيف الالكتروني و القياسات المغناطيسية بأن جميع المعقدات تتخذ شكل المربع المستوي و أن ارتباط الليكاندات (L2 L1) بالايونات الفليزية بشكل ثنائي السن.
Abstract EN
A number of Pd+2 and Pt+2 complexes with 2-methyl-3-aminoquinazoline 4-one (L1) and 2-methyl-3-hydroxyquinazoline-4-one (L2) have been synthesized by direct reaction of Na2PdCl4 or K2PtCl4 with the ligands.
Complexes of the general formula [M(L)(SC6H4.p-Me)2] were also prepared through neucleophilic substitution reaction.
The prepared complexes were characterized by IR and UV / Vis spectroscopy, conductivity, magnetic measurement and the metal content were determined spectrophotometrically.
The electronic spectra and magnetic susceptibility indicates that the complexes have a square planer geometry in which the ligands behave as bidentate.
American Psychological Association (APA)
Izzat, Samir S.. 2008. Synthesis and characterization of palladium (II) and platinum (II) complexes with quinazoline and thiolate derivatives. Rafidain Journal of Science،Vol. 19, no. 2, pp.42-47.
https://search.emarefa.net/detail/BIM-331558
Modern Language Association (MLA)
Izzat, Samir S.. Synthesis and characterization of palladium (II) and platinum (II) complexes with quinazoline and thiolate derivatives. Rafidain Journal of Science Vol. 19, no. 2 (2008), pp.42-47.
https://search.emarefa.net/detail/BIM-331558
American Medical Association (AMA)
Izzat, Samir S.. Synthesis and characterization of palladium (II) and platinum (II) complexes with quinazoline and thiolate derivatives. Rafidain Journal of Science. 2008. Vol. 19, no. 2, pp.42-47.
https://search.emarefa.net/detail/BIM-331558
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 47
Record ID
BIM-331558