Synthesis and characterization complexes of Zn (II), Cd (II), Hg (II) with new schiff base derivative of 4-amino antipyrine with ethylene diamine
Joint Authors
Ghanim, Hasan T.
Muhammad, Mithak S.
Kazim, Afak J.
Source
Journal of Babylon University : Journal of Applied and Pure Sciences
Issue
Vol. 21, Issue 5 (31 Mar. 2013), pp.1674-1680, 7 p.
Publisher
Publication Date
2013-03-31
Country of Publication
Iraq
No. of Pages
7
Main Subjects
Abstract AR
مع ليكاند قاعدة شف المشتقة من 4 – (II) و الزئبق (II) و الكادميوم (II) تضمن البحث تحضير المعقدات لأيونات الخارصين امينو انتييبيرين و 3 – هيدروكسي بنزلديهايد و أثلين ثنائي الأمين.
شخصت المعقدات بوساطة التحليل الدقيق للعناصر و طيف الأشعة تحت الحمراء بالإضافة إلى التوصيلية المولارية و الأطياف الإلكترونية.
بينت نتائج الدراسة أن الليكاند يسلك كليكاند ثلاثية المخلب من تم اقتراح الصيغة التركيبية ثمانية السطوح.
(2:1) و ترتبط مع الأيونات الفلزية مولية (C=N) خلال مجموعة فلز : ليكاند.
Abstract EN
Anew metal complexes of Zn (II), Cd (II) and Hg (II) were synthesized from the Schiff base derived from 4-amino antipyrine, 3-hydroxyl benzaldehyde and ethylene diamine in alcohol medium.
All the complexes were characterized on the basis of their elemental analysis, molar conductance, in addition FTIR and electronic spectra.
The result show that the functional groups was (-C=N).
It has been found that the Schiff base ligand behaves as a tridentate ligand forming chelates with 1:2 (metal : ligand) stoichiometry.
The suggest geometry of the complexes appears to be octahedral.
American Psychological Association (APA)
Muhammad, Mithak S.& Ghanim, Hasan T.& Kazim, Afak J.. 2013. Synthesis and characterization complexes of Zn (II), Cd (II), Hg (II) with new schiff base derivative of 4-amino antipyrine with ethylene diamine. Journal of Babylon University : Journal of Applied and Pure Sciences،Vol. 21, no. 5, pp.1674-1680.
https://search.emarefa.net/detail/BIM-346373
Modern Language Association (MLA)
Kazim, Afak J.…[et al.]. Synthesis and characterization complexes of Zn (II), Cd (II), Hg (II) with new schiff base derivative of 4-amino antipyrine with ethylene diamine. Journal of Babylon University : Journal of Applied and Pure Sciences Vol. 21, no. 5 (2013), pp.1674-1680.
https://search.emarefa.net/detail/BIM-346373
American Medical Association (AMA)
Muhammad, Mithak S.& Ghanim, Hasan T.& Kazim, Afak J.. Synthesis and characterization complexes of Zn (II), Cd (II), Hg (II) with new schiff base derivative of 4-amino antipyrine with ethylene diamine. Journal of Babylon University : Journal of Applied and Pure Sciences. 2013. Vol. 21, no. 5, pp.1674-1680.
https://search.emarefa.net/detail/BIM-346373
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 1679-1680
Record ID
BIM-346373