Effect of surfactants in the synthesis of NiO nanoparticles by colloidal thermal assisted reflux condensation method
Joint Authors
Muhammad Jafar Sadiq M.
Samson Nesaraj A.
Source
Journal of New Technology and Materials
Issue
Vol. 3, Issue 2 (31 Dec. 2013), pp.14-28, 15 p.
Publisher
Larbi Ben M'hidi Oum el-Bouaghi University
Publication Date
2013-12-31
Country of Publication
Algeria
No. of Pages
15
Main Subjects
Topics
Abstract EN
Nickel oxide (NiO) nanoparticles were prepared by colloidal thermal assisted reflux condensation method using nickel acetate (precursor salt) and N, N-Dimethylformamide-DMF (solvent) with or without the addition of surfactants such as cetyl trimethyl ammonium bromide (CTAB), polyvinyl pyrrolidone (PVP), polyvinyl alcohol (PVA) and sodium monododecyl sulphate (SDS) respectively.
Finally, the prepared samples products were calcined at different temperatures systematically such as at 200oC, 400oC, 600oC, 800oC for 2 hrs each to get the phase pure product.
The calcined nanoparticles were characterized by X-Ray Diffraction (XRD), Energy Dispersive X-ray Analysis (EDAX), Fourier Transform Infrared (FTIR) Spectroscopy, Particle Size Analysis, Scanning Electron Microscopy (SEM), Diffuse Reflectance Spectroscopy (DRS) and Photo Luminescence (PL) Spectroscopy techniques.
All the samples were crystallized in cubic structure.
Effect of surfactants in the synthesis of nickel oxide (NiO) particles is discussed and reported.
American Psychological Association (APA)
Muhammad Jafar Sadiq M.& Samson Nesaraj A.. 2013. Effect of surfactants in the synthesis of NiO nanoparticles by colloidal thermal assisted reflux condensation method. Journal of New Technology and Materials،Vol. 3, no. 2, pp.14-28.
https://search.emarefa.net/detail/BIM-368329
Modern Language Association (MLA)
Muhammad Jafar Sadiq M.& Samson Nesaraj A.. Effect of surfactants in the synthesis of NiO nanoparticles by colloidal thermal assisted reflux condensation method. Journal of New Technology and Materials Vol. 3, no. 2 (2013), pp.14-28.
https://search.emarefa.net/detail/BIM-368329
American Medical Association (AMA)
Muhammad Jafar Sadiq M.& Samson Nesaraj A.. Effect of surfactants in the synthesis of NiO nanoparticles by colloidal thermal assisted reflux condensation method. Journal of New Technology and Materials. 2013. Vol. 3, no. 2, pp.14-28.
https://search.emarefa.net/detail/BIM-368329
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 26-28
Record ID
BIM-368329