Uncatalyzed thermal synthesis of new 1,2,3- triazole derivaties

Abstract EN

Two of new Azide and two of new 1, 2, 3-triazole compounds were synthesized.

The triazole compound was prepared by 1,3-dipolar cycloaddition reaction of azido sulfacetmide and azido sulfamethazin with acetylene dicarboxylic acid in acetone as a solvents under reflux condition without catylest.

The reaction mixture was followed by TLC and the yields of products following columgromotography.

IR, H-NMR and Mass spectroscopes were used for the identification of prepared compounds.