Uncatalyzed thermal synthesis of new 1,2,3- triazole derivaties
Joint Authors
al-Mashal, Fayizah A.
Hamid, Nazik
Source
Journal of Basrah Researches : Sciences
Issue
Vol. 40, Issue 1A (31 Mar. 2014), pp.146-159, 14 p.
Publisher
University of Basrah College of Education for Pure Sciences
Publication Date
2014-03-31
Country of Publication
Iraq
No. of Pages
14
Main Subjects
Abstract AR
تخليق اثنين من مركبات الازايدات و اثنين من مركبات 1، 2، 3- ترايازول عن طريق الإضافة الحلقية 1، 3- ثنائية القطب و ذلك بتفاعل ازايدوسلفا استمايد و ازايدو سلفاميثازين مع استلين ثنائي حامض الكاربوكسيلك في الاسيتون كمذيب تحت شروط التصعيد بدون عامل مساعد. تم متابعة التفاعل بواسطة TLC و شخصت المركبات بمطيافية Mass Spectra, 1H.
NMR, IR.
Abstract EN
Two of new Azide and two of new 1, 2, 3-triazole compounds were synthesized.
The triazole compound was prepared by 1,3-dipolar cycloaddition reaction of azido sulfacetmide and azido sulfamethazin with acetylene dicarboxylic acid in acetone as a solvents under reflux condition without catylest.
The reaction mixture was followed by TLC and the yields of products following columgromotography.
IR, H-NMR and Mass spectroscopes were used for the identification of prepared compounds.
American Psychological Association (APA)
al-Mashal, Fayizah A.& Hamid, Nazik. 2014. Uncatalyzed thermal synthesis of new 1,2,3- triazole derivaties. Journal of Basrah Researches : Sciences،Vol. 40, no. 1A, pp.146-159.
https://search.emarefa.net/detail/BIM-371610
Modern Language Association (MLA)
al-Mashal, Fayizah A.& Hamid, Nazik. Uncatalyzed thermal synthesis of new 1,2,3- triazole derivaties. Journal of Basrah Researches : Sciences Vol. 40, no. 1A (Mar. 2014), pp.146-159.
https://search.emarefa.net/detail/BIM-371610
American Medical Association (AMA)
al-Mashal, Fayizah A.& Hamid, Nazik. Uncatalyzed thermal synthesis of new 1,2,3- triazole derivaties. Journal of Basrah Researches : Sciences. 2014. Vol. 40, no. 1A, pp.146-159.
https://search.emarefa.net/detail/BIM-371610
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references : p. 159
Record ID
BIM-371610