Synthesis and characterization of new seven-membered heterocyclic compounds from reaction of new schiff-bases with maleic and phthalic anhydrides

Author

Hannun, Haytham Dalol

Source

National Journal of Chemistry

Issue

Vol. 2011, Issue 41 (31 Mar. 2011), pp.77-89, 13 p.

Publisher

University of Babylon College of Sciences

Publication Date

2011-03-31

Country of Publication

Iraq

No. of Pages

13

Main Subjects

Chemistry

Abstract AR

تم تحضير عدد من قواعد شيف الجديدة و مركبات 3،1- أكسيجين بتكاثف المركب 4- أمينوفينازون مع الديهايدات مختلفة بوجود حامض الخليك الثلجي كعامل مساعد تم الحصول على قواعد شيف [4-2].

فوعلت قواعد شيف هذه مع انهدريد الماليك و أنهدريد الفثاليك في البنزين الجاف فأعطت مشتقات سباعية الحلقة غير متجانسة (5-7) و (8-10) على التوالي.

شخصت جميع المركبات المحضرة باستخدام درجات انصهارها غير المصححة و تحليل العناصر الدقيق و أطياف الأشعة تحت حمراء.

Abstract EN

A series of new Schiff base and 1,3-Oxazepine compounds have been synthesized.

4-Aminophenazone was condensed with various aromatic aldehydes in ethanol in the presence of glacial acetic acid as catalyst to yield the Schiff base [2-4].

These Schiff bases were reacted with maleic anhydride and phthalic anhydride in dry benzene to give a seven-membered heterocyclic ring derivatives [5-7] and [8-10], respectively.

The prepared compounds were identified by their uncorrected melting points, elemental analysis and FT-IR spectra.

American Psychological Association (APA)

Hannun, Haytham Dalol. 2011. Synthesis and characterization of new seven-membered heterocyclic compounds from reaction of new schiff-bases with maleic and phthalic anhydrides. National Journal of Chemistry،Vol. 2011, no. 41, pp.77-89.
https://search.emarefa.net/detail/BIM-405879

Modern Language Association (MLA)

Hannun, Haytham Dalol. Synthesis and characterization of new seven-membered heterocyclic compounds from reaction of new schiff-bases with maleic and phthalic anhydrides. National Journal of Chemistry No. 41 (2011), pp.77-89.
https://search.emarefa.net/detail/BIM-405879

American Medical Association (AMA)

Hannun, Haytham Dalol. Synthesis and characterization of new seven-membered heterocyclic compounds from reaction of new schiff-bases with maleic and phthalic anhydrides. National Journal of Chemistry. 2011. Vol. 2011, no. 41, pp.77-89.
https://search.emarefa.net/detail/BIM-405879

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references : p. 89

Record ID

BIM-405879