Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1)‎ through a Novel Synthetic Rote for Styphnic Acid

Joint Authors

Saad, Hossam A.
Yeşilel, Okan Zafer
Adam, Abdel Majid A.
El-Sayed, Mohamed Y.
Refat, Moamen S.
Taş, Murat

Source

Journal of Chemistry

Issue

Vol. 2013, Issue 2013 (31 Dec. 2013), pp.1-8, 8 p.

Publisher

Hindawi Publishing Corporation

Publication Date

2013-08-18

Country of Publication

Egypt

No. of Pages

8

Main Subjects

Chemistry

Abstract EN

The chemical preparation and crystal structure of styphnic acid and naphthalene-1,4-diol (1 : 1) (I) have been reported.

The compound crystallizes in the orthorhombic system in space group Pnma and cell parameters a=6.6712(2), b=16.8267(7), c=13.6450(5) Å and V=1531.71(10) Å3, and Z=4.

Crystal structure has been determined and refined to R=0.0576.

The crystal structure of I, the asymmetric unit, contains C6H2N3O7, C10H7O, and it is a half portion of both styphnic acid and naphthalene-1,4-diol.

The O1–H1⋯O2 intramolecular hydrogen bond was found between the O–H and a nitro group in the styphnic acid unit.

American Psychological Association (APA)

Refat, Moamen S.& Saad, Hossam A.& El-Sayed, Mohamed Y.& Adam, Abdel Majid A.& Yeşilel, Okan Zafer& Taş, Murat. 2013. Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid. Journal of Chemistry،Vol. 2013, no. 2013, pp.1-8.
https://search.emarefa.net/detail/BIM-446980

Modern Language Association (MLA)

Refat, Moamen S.…[et al.]. Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid. Journal of Chemistry No. 2013 (2013), pp.1-8.
https://search.emarefa.net/detail/BIM-446980

American Medical Association (AMA)

Refat, Moamen S.& Saad, Hossam A.& El-Sayed, Mohamed Y.& Adam, Abdel Majid A.& Yeşilel, Okan Zafer& Taş, Murat. Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid. Journal of Chemistry. 2013. Vol. 2013, no. 2013, pp.1-8.
https://search.emarefa.net/detail/BIM-446980

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references

Record ID

BIM-446980