Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid
Joint Authors
Saad, Hossam A.
Yeşilel, Okan Zafer
Adam, Abdel Majid A.
El-Sayed, Mohamed Y.
Refat, Moamen S.
Taş, Murat
Source
Issue
Vol. 2013, Issue 2013 (31 Dec. 2013), pp.1-8, 8 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2013-08-18
Country of Publication
Egypt
No. of Pages
8
Main Subjects
Abstract EN
The chemical preparation and crystal structure of styphnic acid and naphthalene-1,4-diol (1 : 1) (I) have been reported.
The compound crystallizes in the orthorhombic system in space group Pnma and cell parameters a=6.6712(2), b=16.8267(7), c=13.6450(5) Å and V=1531.71(10) Å3, and Z=4.
Crystal structure has been determined and refined to R=0.0576.
The crystal structure of I, the asymmetric unit, contains C6H2N3O7, C10H7O, and it is a half portion of both styphnic acid and naphthalene-1,4-diol.
The O1–H1⋯O2 intramolecular hydrogen bond was found between the O–H and a nitro group in the styphnic acid unit.
American Psychological Association (APA)
Refat, Moamen S.& Saad, Hossam A.& El-Sayed, Mohamed Y.& Adam, Abdel Majid A.& Yeşilel, Okan Zafer& Taş, Murat. 2013. Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid. Journal of Chemistry،Vol. 2013, no. 2013, pp.1-8.
https://search.emarefa.net/detail/BIM-446980
Modern Language Association (MLA)
Refat, Moamen S.…[et al.]. Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid. Journal of Chemistry No. 2013 (2013), pp.1-8.
https://search.emarefa.net/detail/BIM-446980
American Medical Association (AMA)
Refat, Moamen S.& Saad, Hossam A.& El-Sayed, Mohamed Y.& Adam, Abdel Majid A.& Yeşilel, Okan Zafer& Taş, Murat. Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid. Journal of Chemistry. 2013. Vol. 2013, no. 2013, pp.1-8.
https://search.emarefa.net/detail/BIM-446980
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-446980