Synthesis and Conformational Assignment of N-(E)‎-Stilbenyloxymethylenecarbonyl-Substituted Hydrazones of Acetone and o-(m- and p-)‎ Chloro- (nitro-)‎ benzaldehydes by Means of H1 and C13 NMR Spectroscopy

Joint Authors

Wyrzykiewicz, Elżbieta
Bartkowiak, Grażyna
Patorski, Przemysław

Source

Journal of Spectroscopy

Issue

Vol. 2013, Issue 2013 (31 Dec. 2013), pp.1-12, 12 p.

Publisher

Hindawi Publishing Corporation

Publication Date

2012-12-31

Country of Publication

Egypt

No. of Pages

12

Main Subjects

Physics

Abstract EN

Eighteen new N-(E)-stilbenyloxyalkylcarbonyl-substituted hydrazones of ortho- (meta- and para-) chloro- (nitro-) benzaldehydes 1–18 and two analogous hydrazones of acetone 19-20 were prepared.

The stereochemical behavior of 1–18 in dimethyl-d6 sulfoxide solution has been studied by H1 NMR and C13 NMR techniques, using spectral data of 19 and 20 as supporting material.

The E-geometrical isomers and cis-/trans-amide conformers have been found for these hydrazones.

Energy barriers of isomers are reported.

American Psychological Association (APA)

Patorski, Przemysław& Wyrzykiewicz, Elżbieta& Bartkowiak, Grażyna. 2012. Synthesis and Conformational Assignment of N-(E)-Stilbenyloxymethylenecarbonyl-Substituted Hydrazones of Acetone and o-(m- and p-) Chloro- (nitro-) benzaldehydes by Means of H1 and C13 NMR Spectroscopy. Journal of Spectroscopy،Vol. 2013, no. 2013, pp.1-12.
https://search.emarefa.net/detail/BIM-453799

Modern Language Association (MLA)

Patorski, Przemysław…[et al.]. Synthesis and Conformational Assignment of N-(E)-Stilbenyloxymethylenecarbonyl-Substituted Hydrazones of Acetone and o-(m- and p-) Chloro- (nitro-) benzaldehydes by Means of H1 and C13 NMR Spectroscopy. Journal of Spectroscopy No. 2013 (2013), pp.1-12.
https://search.emarefa.net/detail/BIM-453799

American Medical Association (AMA)

Patorski, Przemysław& Wyrzykiewicz, Elżbieta& Bartkowiak, Grażyna. Synthesis and Conformational Assignment of N-(E)-Stilbenyloxymethylenecarbonyl-Substituted Hydrazones of Acetone and o-(m- and p-) Chloro- (nitro-) benzaldehydes by Means of H1 and C13 NMR Spectroscopy. Journal of Spectroscopy. 2012. Vol. 2013, no. 2013, pp.1-12.
https://search.emarefa.net/detail/BIM-453799

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references

Record ID

BIM-453799