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Synthesis and Spectroscopic Studies of Some New Molybdenum, Tungsten, and Ruthenium Carbonyl Derivatives of 2-Hydroxymethylpyridine
Joint Authors
Ramadan, R. M.
Jarelnabbi, S. E.
Bayoumy, B. E.
El-Medani, S. M.
Taher, M. A.
Source
International Journal of Inorganic Chemistry
Issue
Vol. 2010, Issue 2010 (31 Dec. 2010), pp.1-6, 6 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2010-02-23
Country of Publication
Egypt
No. of Pages
6
Main Subjects
Abstract EN
Thermal reactions of 2-hydroxymethylpyridine (HMP) with [M(CO)6] in air resulted in formation of the oxo-complexes [M2O6(HMP)2], where M = Mo, 1, or W, 2.
The tricarbonyl complex [Ru(CO)3(HMP)], 3, was obtained from the reaction of [Ru3(CO)12] with HMP.
In presence of triphenyl phosphine (PPh3), the reaction of HMP with Ru3(CO)12 gave [Ru(CO)2(HMP)(PPh3)], 4.
All the complexes were characterized by elemental analysis, mass spectrometry, IR, and NMR spectroscopy.
The thermal properties of the complexes were also investigated by thermogravimetry technique.
American Psychological Association (APA)
Taher, M. A.& Jarelnabbi, S. E.& Bayoumy, B. E.& El-Medani, S. M.& Ramadan, R. M.. 2010. Synthesis and Spectroscopic Studies of Some New Molybdenum, Tungsten, and Ruthenium Carbonyl Derivatives of 2-Hydroxymethylpyridine. International Journal of Inorganic Chemistry،Vol. 2010, no. 2010, pp.1-6.
https://search.emarefa.net/detail/BIM-461301
Modern Language Association (MLA)
Taher, M. A.…[et al.]. Synthesis and Spectroscopic Studies of Some New Molybdenum, Tungsten, and Ruthenium Carbonyl Derivatives of 2-Hydroxymethylpyridine. International Journal of Inorganic Chemistry No. 2010 (2010), pp.1-6.
https://search.emarefa.net/detail/BIM-461301
American Medical Association (AMA)
Taher, M. A.& Jarelnabbi, S. E.& Bayoumy, B. E.& El-Medani, S. M.& Ramadan, R. M.. Synthesis and Spectroscopic Studies of Some New Molybdenum, Tungsten, and Ruthenium Carbonyl Derivatives of 2-Hydroxymethylpyridine. International Journal of Inorganic Chemistry. 2010. Vol. 2010, no. 2010, pp.1-6.
https://search.emarefa.net/detail/BIM-461301
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-461301