Effect of Synthesis Temperature on the Growth Iron-Filled Carbon Nanotubes as Evidenced by Structural, Micro-Raman, and Thermogravimetric Analyses

Abstract EN

Tubular structure and well dense of aligned carbon nanotubes (CNTs) were formulated using two-stage catalytic chemical vapor deposition apparatus.

In this experiment, aligned CNT was synthesized in the range of 700–900°C temperatures with increment rate of 50°C per sample.

The aligned CNT properties were investigated via field emission scanning electron microscope, micro-Raman spectrometer and thermogravimetric analyzer.

The experimental results showed that aligned CNT properties were highly dependent on synthesis temperature changes.

The optimum temperature of higher crystallinity was observed at 800°C synthesis temperature.

However, the highest yield of nanotubes (~99.99%) was obtained at 900°C synthesis temperature.

Aligned CNT orientation was in a parallel form and packed together in orderly manner.

The behaviors of aligned CNT will be discussed in detail in this paper.