Microwave-Assisted Synthesis of Arylidene Acetophenones
Joint Authors
Khatun, Khodeza
Khan, M. Z. H.
Sattar, M. A.
Khatun, Sheauly
Source
Issue
Vol. 2013, Issue 2013 (31 Dec. 2013), pp.1-5, 5 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2013-06-24
Country of Publication
Egypt
No. of Pages
5
Main Subjects
Abstract EN
An efficient synthesis of arylidene acetophenones have been achieved by using the microwave heating in comparison to the conventional heating.
In this work compound 1-phenyle-3-(4-droxyphenyle)-2-propen-1-one, 1-(4-chlorophenyle)-3-phenyle-2-propen-1-one, and 1-(4-chlorophenyle)-3-(4-hydroxyphenyle)-2-propen-1-one have been synthesized by the condensation reaction between aromatic aldehydes and substituted acetophenones under microwave irradiation.
The compounds of aldehydes and acetophenones were used as benzaldehyde, parahydroxybenzaldehyde, acetophenone, and parachloroacetophenone.
The result shows that the time taken for the reaction was reduced from the conventional 1-2 hours to 60–120 seconds.
The yield of the compounds in the conventional heating was moderate while the highest yield of 90–98% was observed in MWI method.
The structure of the compounds was characterized by their IR, 1H-NMR spectral data.
American Psychological Association (APA)
Khatun, Sheauly& Khan, M. Z. H.& Khatun, Khodeza& Sattar, M. A.. 2013. Microwave-Assisted Synthesis of Arylidene Acetophenones. Journal of Engineering،Vol. 2013, no. 2013, pp.1-5.
https://search.emarefa.net/detail/BIM-471617
Modern Language Association (MLA)
Khatun, Sheauly…[et al.]. Microwave-Assisted Synthesis of Arylidene Acetophenones. Journal of Engineering No. 2013 (2013), pp.1-5.
https://search.emarefa.net/detail/BIM-471617
American Medical Association (AMA)
Khatun, Sheauly& Khan, M. Z. H.& Khatun, Khodeza& Sattar, M. A.. Microwave-Assisted Synthesis of Arylidene Acetophenones. Journal of Engineering. 2013. Vol. 2013, no. 2013, pp.1-5.
https://search.emarefa.net/detail/BIM-471617
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-471617