Synthesis, Crystal Growth, Spectroscopic and Electrical Properties of 5-tert-Butyl-1,2,3-trinitrobenzene
Joint Authors
Nayak, M. Muralidhar
Dhas, S. A. Martin Britto
Dhas, S. Sahaya Jude
Jerome Das, S.
Source
Issue
Vol. 2013, Issue 2013 (31 Dec. 2013), pp.1-6, 6 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2013-02-26
Country of Publication
Egypt
No. of Pages
6
Main Subjects
Materials Science , Minerals
Civil Engineering
Abstract EN
5-tert-Butyl-1,2,3-trinitrobenzene (TBTB) was synthesized and characterized by NMR so as to confirm the structure.
Single crystals were obtained from methanol by solvent evaporation technique at room temperature.
Optically transparent single crystals with dimension up to 17×4×3 mm3 have been grown by submerged seed solution method within a period of 30 days.
The modes of vibration of different molecular groups present in the title compound were identified by FTIR and FT-Raman spectral analyses, and it was found with the tabulation that both of the spectral vibrations are very close to each other confirming the existence of specific functional groups in the crystal.
Optical behaviour of the crystal was analyzed by UV-Vis absorption studies, and the value of the optical band gap energy (Eg) of the crystal has been determined using the optical absorption spectrum.
The dielectric behaviour and AC conductivity of the grown crystals were also analyzed, and it is shown that both properties vary with respect to frequency and do not vary in accordance with temperature.
American Psychological Association (APA)
Dhas, S. Sahaya Jude& Nayak, M. Muralidhar& Jerome Das, S.& Dhas, S. A. Martin Britto. 2013. Synthesis, Crystal Growth, Spectroscopic and Electrical Properties of 5-tert-Butyl-1,2,3-trinitrobenzene. Journal of Materials،Vol. 2013, no. 2013, pp.1-6.
https://search.emarefa.net/detail/BIM-480844
Modern Language Association (MLA)
Dhas, S. Sahaya Jude…[et al.]. Synthesis, Crystal Growth, Spectroscopic and Electrical Properties of 5-tert-Butyl-1,2,3-trinitrobenzene. Journal of Materials No. 2013 (2013), pp.1-6.
https://search.emarefa.net/detail/BIM-480844
American Medical Association (AMA)
Dhas, S. Sahaya Jude& Nayak, M. Muralidhar& Jerome Das, S.& Dhas, S. A. Martin Britto. Synthesis, Crystal Growth, Spectroscopic and Electrical Properties of 5-tert-Butyl-1,2,3-trinitrobenzene. Journal of Materials. 2013. Vol. 2013, no. 2013, pp.1-6.
https://search.emarefa.net/detail/BIM-480844
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-480844