Simultaneous Determination of Parathion, Malathion, Diazinon, and Pirimiphos Methyl in Dried Medicinal Plants Using Solid-Phase Microextraction Fibre Coated with Single-Walled Carbon Nanotubes
Joint Authors
Ahmadkhaniha, Reza
Samadi, Nasrin
Salimi, Mona
Sarkhail, Parisa
Rastkari, Noushin
Source
Issue
Vol. 2012, Issue 2012 (31 Dec. 2012), pp.1-8, 8 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2012-05-02
Country of Publication
Egypt
No. of Pages
8
Main Subjects
Natural & Life Sciences (Multidisciplinary)
Medicine
Information Technology and Computer Science
Abstract EN
A reliable and sensitive headspace solid-phase microextraction gas chromatography-mass spectrometry method for simultaneous determination of different organophosphorus pesticides in dried medicinal plant samples is described.
The analytes were extracted by single-walled carbon nanotubes as a new solid-phase microextraction adsorbent.
The developed method showed good performance.
For diazinon and pirimiphos methyl calibration, curves were linear (r2≥0.993) over the concentration ranges from 1.5 to 300 ng g−1, and the limit of detection at signal-to-noise ratio of 3 was 0.3 ng g−1.
For parathion and malathion, the linear range and limit of detection were 2.5–300 (r2≥0.991) and 0.5 ng g−1, respectively.
In addition, a comparative study between the single-walled carbon nanotubes and a commercial polydimethylsiloxane fibre for the determination of target analytes was carried out.
Single-walled carbon nanotubes fibre showed higher extraction capacity, better thermal stability (over 350∘C), and longer lifespan (over 250 times) than the commercial polydimethylsiloxane fibre.
The developed method was successfully applied to determine target organophosphorus pesticides in real samples.
American Psychological Association (APA)
Ahmadkhaniha, Reza& Samadi, Nasrin& Salimi, Mona& Sarkhail, Parisa& Rastkari, Noushin. 2012. Simultaneous Determination of Parathion, Malathion, Diazinon, and Pirimiphos Methyl in Dried Medicinal Plants Using Solid-Phase Microextraction Fibre Coated with Single-Walled Carbon Nanotubes. The Scientific World Journal،Vol. 2012, no. 2012, pp.1-8.
https://search.emarefa.net/detail/BIM-486307
Modern Language Association (MLA)
Ahmadkhaniha, Reza…[et al.]. Simultaneous Determination of Parathion, Malathion, Diazinon, and Pirimiphos Methyl in Dried Medicinal Plants Using Solid-Phase Microextraction Fibre Coated with Single-Walled Carbon Nanotubes. The Scientific World Journal No. 2012 (2012), pp.1-8.
https://search.emarefa.net/detail/BIM-486307
American Medical Association (AMA)
Ahmadkhaniha, Reza& Samadi, Nasrin& Salimi, Mona& Sarkhail, Parisa& Rastkari, Noushin. Simultaneous Determination of Parathion, Malathion, Diazinon, and Pirimiphos Methyl in Dried Medicinal Plants Using Solid-Phase Microextraction Fibre Coated with Single-Walled Carbon Nanotubes. The Scientific World Journal. 2012. Vol. 2012, no. 2012, pp.1-8.
https://search.emarefa.net/detail/BIM-486307
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-486307