Optimization of SPEGCHPLC Analytical Procedure for Determination of Phenol, Quinones, and Carboxylic Acids in Water Samples
Joint Authors
Voelkel, Adam
Bielicka-Daszkiewicz, Katarzyna
Hadzicka, Monika
Source
Issue
Vol. 2012, Issue 2012 (31 Dec. 2012), pp.1-7, 7 p.
Publisher
Hindawi Publishing Corporation
Publication Date
2012-06-18
Country of Publication
Egypt
No. of Pages
7
Main Subjects
Abstract EN
Chromatographic techniques are among the most useful analytical methods.
Gas and liquid chromatography were used in the analysis of some organic compounds: phenol, hydroquinone, benzoquinone, and maleic and fumaric acids.
The analytical way for the determination of these compounds in water samples was investigated.
Solid-phase extraction (SPE) technique was used on the sample preparation step, different divinylbenzene-based sorbents were applied.
Calibration curves of given compounds were linear over the ranges: 50–500 μg/mL for phenol and its acetic derivatives, 50–1500 μg/mL for benzoquinone in GC analysis, and 50–250 μg/mL for phenol, 40–1000 μg/mL for hydroquinone, and 4–4500 μg/mL for carboxylic acids in HPLC analysis.
The LOD and LOQ of proposed analytical procedure were in the ranges of LOD: 0.042–23.83 μg/mL; LOQ: 0.138–78.64 μg/mL.
American Psychological Association (APA)
Bielicka-Daszkiewicz, Katarzyna& Hadzicka, Monika& Voelkel, Adam. 2012. Optimization of SPEGCHPLC Analytical Procedure for Determination of Phenol, Quinones, and Carboxylic Acids in Water Samples. ISRN Chromatography،Vol. 2012, no. 2012, pp.1-7.
https://search.emarefa.net/detail/BIM-490025
Modern Language Association (MLA)
Bielicka-Daszkiewicz, Katarzyna…[et al.]. Optimization of SPEGCHPLC Analytical Procedure for Determination of Phenol, Quinones, and Carboxylic Acids in Water Samples. ISRN Chromatography No. 2012 (2012), pp.1-7.
https://search.emarefa.net/detail/BIM-490025
American Medical Association (AMA)
Bielicka-Daszkiewicz, Katarzyna& Hadzicka, Monika& Voelkel, Adam. Optimization of SPEGCHPLC Analytical Procedure for Determination of Phenol, Quinones, and Carboxylic Acids in Water Samples. ISRN Chromatography. 2012. Vol. 2012, no. 2012, pp.1-7.
https://search.emarefa.net/detail/BIM-490025
Data Type
Journal Articles
Language
English
Notes
Includes bibliographical references
Record ID
BIM-490025