Rapid Synthesis and Characterization of an Oxygen-Deficient Defect Perovskite La4BaCu5O13+δ Phase

Author

Shivakumara, Chikkadasappa

Source

ISRN Ceramics

Issue

Vol. 2011, Issue 2011 (31 Dec. 2011), pp.1-4, 4 p.

Publisher

Hindawi Publishing Corporation

Publication Date

2011-10-13

Country of Publication

Egypt

No. of Pages

4

Main Subjects

Civil Engineering

Abstract EN

Oxygen-deficient defect perovskite La4BaCu5O13+δ phase has been synthesized by the nitrate-citrate gel combustion method at 950°C for 2 h.

Structural parameters were refined by the Rietveld refinement method using room-temperature powder XRD data.

The La4BaCu5O13+δ crystallizes in the tetragonal structure with space group P4/m (no.

83) and having the lattice parameters a=8.6508(1) Å and c=3.8606(2) Å, respectively.

Oxygen content was determined by the iodometric titration.

Low-temperature resistivity result reveals that La4BaCu5O13+δ compound exhibit metallic behavior up to 15 K.

American Psychological Association (APA)

Shivakumara, Chikkadasappa. 2011. Rapid Synthesis and Characterization of an Oxygen-Deficient Defect Perovskite La4BaCu5O13+δ Phase. ISRN Ceramics،Vol. 2011, no. 2011, pp.1-4.
https://search.emarefa.net/detail/BIM-503994

Modern Language Association (MLA)

Shivakumara, Chikkadasappa. Rapid Synthesis and Characterization of an Oxygen-Deficient Defect Perovskite La4BaCu5O13+δ Phase. ISRN Ceramics No. 2011 (2011), pp.1-4.
https://search.emarefa.net/detail/BIM-503994

American Medical Association (AMA)

Shivakumara, Chikkadasappa. Rapid Synthesis and Characterization of an Oxygen-Deficient Defect Perovskite La4BaCu5O13+δ Phase. ISRN Ceramics. 2011. Vol. 2011, no. 2011, pp.1-4.
https://search.emarefa.net/detail/BIM-503994

Data Type

Journal Articles

Language

English

Notes

Includes bibliographical references

Record ID

BIM-503994